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首页> 外文期刊>Journal of cluster science >Preparation of Ag Nanoparticles in Ammonia by Using EDM and a Study of the Relationships Between Ammonia and Silver Nanoparticles
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Preparation of Ag Nanoparticles in Ammonia by Using EDM and a Study of the Relationships Between Ammonia and Silver Nanoparticles

机译:用EDM制备氨中的Ag纳米颗粒及氨与银纳米粒子关系的研究

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摘要

This study used deionized water and ammonia (0.02%) as dielectric fluids and then employed electronic discharge machine to ionize them, with the arc-focused energy melting the surface of silver electrode rods. After the condensation of the dielectric fluid, silver nano-colloids were prepared under two conditions, named as Ag and Ag(NH3), respectively. The optical properties of the two samples were compared by a UV-Vis spectrum analyzer (UV-Vis), and the zeta potential was measured by Zetasizer. We then utilized a transmission electron microscope to observe the shape, size, and distribution of silver nanoparticles. The results showed that with the addition of NH3, the size of silver nanoparticles decreased, the concentration of nano-colloid increased, and the dispersive suspension of nano-colloid became better.
机译:该研究使用去离子水和氨(0.02%)作为介电流流体,然后采用电子放电机电,以电弧能量熔化银电极棒的表面。 在介电流体冷凝后,在两个条件下,分别在两个条件下制备银纳米胶体,分别被命名为Ag和Ag(NH3)。 通过UV-Vis谱分析仪(UV-VI)进行比较两个样品的光学性质,并通过Zetasizer测量Zeta电位。 然后,我们利用透射电子显微镜观察银纳米粒子的形状,尺寸和分布。 结果表明,随着NH 3的添加,银纳米粒子的尺寸降低,纳米胶体的浓度增加,纳米胶体的分散悬浮液变得更好。

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