Tin powder-promoted allylation and cyclization of 2-(benzylideneamino)isoindoline-1,3-diones

Nibras AhmedElaas; DanfengHuang; Ke-HuWang; YingpengSu; YulaiHu

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Tin powder-promoted allylation and cyclization of 2-(benzylideneamino)isoindoline-1,3-diones

机译：锡粉 - 促进的烯丙基化和2-（苄基氨基）异吲哚-1,3-致力的环化

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摘要

α-Methylene-γ-lactams were synthesized from readily available N-acylhydrazones by a tin-mediated Barbier-type reaction. The method avoids the use of toxic allylstannanes and the reaction proceeds smoothly under mild conditions.

机译：通过锡介导的倒钩型反应从易于可获得的N-酰基缺水合成α-甲基-γ-内酰胺。该方法避免使用有毒烯丙基烷烃，并且反应在温和条件下平稳地进行。

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来源
《Heterocyclic communications》 |2018年第3期|共5页
作者
Nibras AhmedElaas; DanfengHuang; Ke-HuWang; YingpengSu; YulaiHu;
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作者单位

College of Chemistry and Chemical Engineering Northwest Normal University Lanzhou 730070 China;

College of Chemistry and Chemical Engineering Northwest Normal University Lanzhou 730070 China;

College of Chemistry and Chemical Engineering Northwest Normal University Lanzhou 730070 China;

College of Chemistry and Chemical Engineering Northwest Normal University Lanzhou 730070 China;

College of Chemistry and Chemical Engineering Northwest Normal University Lanzhou 730070 China;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
allylation; homoallylic N-aminophthalimide; lactam; tin powder;

机译：allylation;同性恋n-氨基酰亚胺;内酰胺;锡粉;

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专利

1. Tin powder-promoted allylation and cyclization of 2-(benzylideneamino)isoindoline-1,3-diones [J] . Nibras AhmedElaas, DanfengHuang, Ke-HuWang, Heterocyclic communications . 2018,第3期

机译：锡粉 - 促进的烯丙基化和2-（苄基氨基）异吲哚-1,3-致力的环化
2. Simple method for synthesis of isolated heterocyclic compounds incorporating 2-(2-bromoacetyl)isoindoline-1,3-dione and 2-(2-cyanoacetyl)isoindoline-1,3-dione [J] . Islam Helmy El Azab, Eman Abd El Rady Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2014,第9期

机译：合成2-（2-溴乙酰基）异吲哚啉-1,3-二酮和2-（2-氰基乙酰基）异吲哚啉-1,3-二酮的分离的杂环化合物的简单方法
3. Photocleavage Properties and DNA-Binding Studies of Oxovanadium Complexes Incorporating 2-(2-Hydroxybenzylideneamino) Isoindoline-1,3-Dione and Fluoro-Phenanthroline Derivatives [J] . Peng Ying, Pengfei Zeng, Jiazheng Lu, Open Journal of Inorganic Chemistry . 2014,第4期

机译：含2-（2-羟基苄叉亚氨基）异吲哚啉-1,3-二酮和氟代邻菲咯啉衍生物的氧钒络合物的光解性质和DNA结合研究
4. Synthesis of Nitrogen Heterocycles via Amphiphilic Allylation of Aldimine [C] . Katsumi Tohyama, Daisuke Nojiri, Masanari Kimura Symposium on Organometallic Chemistry . 2008

机译：通过醛胺的两亲烯丙基合成氮杂杂环
5. Palladium- and ruthenium-catalyzed decarboxylative allylations and Michael addition -allylation reactions. Applications in nitrogen heterocycle synthesis [D] . Wang, Chao 2008

机译：钯和钌催化的脱羧烯丙基化和迈克尔加成-烯丙基化反应。在氮杂环合成中的应用
6. 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate [O] . Zhen Wei, Jinlong Guo, Xujun Zheng, 2015

机译：3′，6′-双（二乙基氨基）-2-[（E）-2-（4-羟基-3-氧基苄叉亚基氨基）乙基]螺spir [异吲哚啉-1,9'-黄嘌呤] -3-一乙醇单溶剂化物
7. Photocleavage Properties and DNA-Binding Studies of Oxovanadium Complexes Incorporating 2-(2-Hydroxybenzylideneamino) Isoindoline-1,3-Dione and Fluoro-Phenanthroline Derivatives [O] . Peng Ying, Pengfei Zeng, Jiazheng Lu, 2014

机译：掺入2-（2-羟基苄基氨基）异吲哚-1,3-二酮和氟 - 菲咯啉衍生物的氧化钒络合物的光敏性和DNA结合研究

Tin powder-promoted allylation and cyclization of 2-(benzylideneamino)isoindoline-1,3-diones

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