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Synthesis of Nanoalumina/Graphene Oxide Hybrid for Improvement Tribological Property of Aluminum

机译:铝合金改善摩擦族氧化物杂种氧化物氧化物杂种的合成

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摘要

In this research, an efficient, facile and low-cost chemical method was the developed for preparation of Al(2)O(3/)graphene oxide (GO) hybrid nanoparticle (Al(2)O(3)Nps/GO), through in situ synthesis of Al(2)O(3)Nps in the presence of GO. Al(2)O(3)Nps/GO hybrid nanoparticles added to aluminum powder and nanocomposites were fabricated by powder metallurgy processing and consolidated via the spark plasma sintering. Structure, morphology and composition of the hybrid particle were investigated by means of X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy, Raman spectra and thermogravimetric analysis. The results confirmed successful incorporation of alumina over GO surface and formation of pure and homogenized gamma-Al(2)O(3)Nps/GO hybrid particle. Physical and tribological properties of hybrid nanocomposite were investigated by using density, hardness and wear analyses. High relative density was obtained for Al 1 wt% gamma-Al(2)O(3)Nps/GO. Tribological property was studied by pin-on-disk tribometer and showed that the friction coefficient significantly decreased with increasing gamma-Al(2)O(3)Nps/GO content.
机译:在本研究中,高效,容易和低成本的化学方法是制备Al(2)O(3 /)石墨烯氧化物(GO)杂化纳米粒子(Al(2)O(3)NPS / Go)的制备,通过在GO的情况下原位合成Al(2)O(3)NPS。通过粉末冶金加工制备添加到铝粉末和纳米复合材料中的NPS / GO杂化纳米颗粒,并通过火花等离子体烧结固结。通过X射线衍射,扫描电子显微镜,能量分散X射线光谱,拉曼光谱和热重分析来研究杂化颗粒的结构,形态和组成。结果证实,成功掺入氧化铝过度表面并形成纯净和均质γ-Al(2)O(3)NPS / GO杂化颗粒。利用密度,硬度和磨损分析研究了杂化纳米复合材料的物理和摩擦学特性。对于Al 1wt%γ-Al(2)O(3)NPS / GO,获得高相对密度。通过焊盘摩擦计研究摩擦学性质,并显示摩擦系数随着γ-Al(2)O(3)NPS / GO含量的增加而显着降低。

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