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Synthesis and characterization of highly dispersed multi-walled carbon nanotubes/polyvinylpyrrolidone composite nanofibers for EMI shielding application

机译:高度分散的多壁碳纳米管/聚乙烯基吡咯烷酮复合纳米纤维的合成与表征,用于EMI屏蔽应用

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Multi-walled carbon nanotubes (MWCNTs)/polyvinylpyrrolidone (PVP) composite nanofibers having varying amounts of MWCNTs were fabricated with an aim to investigate the potential of such nanofibers as an effective light weight electromagnetic interference (EMI) shielding material in the frequency range of 8.2-12.4 GHz (X-band). The state of dispersion of MWCNTs in PVP matrix was studied by transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The TEM and SEM analyses confirmed the presence of individual dispersion MWCNTs encapsulated within the electrospun nanofibers and showed MWCNTs/PVP composite nanofiber morphologies with diameters of 150-600 nm. Moreover, the MWCNTs/PVP composite nanofibers were characterized by X-ray diffraction and Raman spectrophotometer. The thermal stability of composite nanofibers studied from thermogravimetric analysis was increased after addition of MWCNTs to PVP matrix. The EMI shielding efficiency of MWCNTs/PVP composite nanofibers increased up to 42 dB. The MWCNTs/PVP composite nanofibers developed in this study have benefits in being light weight and having effective EMI shielding performance and can be best candidates for a broad range of electronic applications. POLYM. COMPOS., 38:2026-2034, 2017. (c) 2016 Society of Plastics Engineers
机译:具有不同量的MWCNT的多壁碳纳米管(MWCNT)/聚乙烯醇吡咯烷酮(PVP)复合纳米纤维是制造的,旨在研究这种纳米纤维的电位,作为8.2的频率范围内的有效轻型电磁干扰(EMI)屏蔽材料-12.4 GHz(X波段)。通过透射电子显微镜(TEM)和扫描电子显微镜(SEM)研究了MWNTS在PVP基质中的分散状态。 TEM和SEM分析证实存在封装在电纺纳米纤维内的单独分散MWCNT,并显示出直径为150-600nm的MWCNT / PVP复合纳米纤维形态。此外,通过X射线衍射和拉曼分光光度计表征MWCNT / PVP复合纳米纤维。在加入MWCNT至PVP基质后,从热重分析研究的复合纳米纤维的热稳定性增加。 MWCNTS / PVP复合纳米纤维的EMI屏蔽效率高达42 dB。本研究开发的MWCNTS / PVP复合纳米纤维具有重量轻,具有有效的EMI屏蔽性能,并且可以是广泛的电子应用的最佳候选者。聚合物。 Compos。,38:2026-2034,2017。(c)2016年塑料工程师协会

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