Integration of Sequential Reactions in a Continuous Flow Droplet Reactor: A Route to Architecturally Defined Bimetallic Nanostructures

Santana Joshua S.; Gamler Jocelyn T. L.; Skrabalak Sara E.

摘要

Abstract >Microreactors for nanoparticle (NP) synthesis offer advantages over batch reactions in terms of scale‐up and integration with online analyses. Herein, two microreactors (i.e., a duo‐microreactor) are integrated to achieve sequential reactions for the synthesis of bimetallic NPs with architectural control. The generality of the duo‐microreactor is shown with the synthesis of branched Pd‐Pt NPs and core@shell Pd@Au NPs, both achieved by synthesizing Pd nanocubes in the first part of the duo‐microreactor and then using those nanocubes downstream as seeds for Pt or Au deposition. Control of the dimensions of these NPs is further demonstrated and achieved by tailoring metal precursor concentrations inline. This microreactor methodology is anticipated to be applicable to other bimetallic NP systems. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >纳米粒子（NP）合成的微反应器在扩大和与在线分析中的扩展和集成方面提供优于批次反应的优势。这里，两种微反应器（即Duo-MicroreActor）被整合以实现具有建筑控制的双金属NP的顺序反应。通过合成支链Pd-Pt NPS和核心/壳Pd / au nps的合成，通过合成Duo-Micrea反应器的第一部分，然后使用下游的那些纳米孔作为种子来实现的分支Pd-Pt NP和核心壳Pd @ au nps的一般性。对于Pt或au沉积。通过甲状金属前体浓度绕整向剪裁金属前体浓度，进一步证明和实现这些NP的尺寸。预计该微反应器方法可以适用于其他双金属NP系统。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-28901/'>《Particle & Particle Systems Characterization: Measurement and Description of Particle Properties and Behavior in Powders and Other Disperse Systems》</a> <b style="margin: 0 2px;">|</b><span>2019年第9期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Santana Joshua S.&option=202" target="_blank" rel="nofollow">Santana Joshua S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gamler Jocelyn T. L.&option=202" target="_blank" rel="nofollow">Gamler Jocelyn T. L.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Skrabalak Sara E.&option=202" target="_blank" rel="nofollow">Skrabalak Sara E.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryIndiana University800 E. Kirkwood Ave. Bloomington 47405 IN USA;</p> <p>Department of ChemistryIndiana University800 E. Kirkwood Ave. Bloomington 47405 IN USA;</p> <p>Department of ChemistryIndiana University800 E. Kirkwood Ave. Bloomington 47405 IN USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=gold&option=203" rel="nofollow">gold;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanodendrites&option=203" rel="nofollow">nanodendrites;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=palladium&option=203" rel="nofollow">palladium;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=platinum&option=203" rel="nofollow">platinum;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=seeded synthesis&option=203" rel="nofollow">seeded synthesis;</a> </p> <div class="translation"> 机译：金;纳秒;钯;铂;种子合成; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024384468.html">Integration of Sequential Reactions in a Continuous Flow Droplet Reactor: A Route to Architecturally Defined Bimetallic Nanostructures</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Santana Joshua S.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Santana Joshua S.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gamler Jocelyn T. 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SYSTEM</a> <b>[P]</b> . <span> 外国专利：  RU2726178C1 </span> <span> . 2020-07-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：管流偏转室，连续流反应器和带有控制系统的连续流反应系统 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130400262326.html">PIPE FLOW DEFLECTION CHAMBER, CONTINUOUS FLOW REACTOR AND CONTINUOUS FLOW REACTION SYSTEM WITH CONTROL SYSTEM</a> <b>[P]</b> . <span> 外国专利：  RU0002726178C1 </span> <span> . 2020.07.09</span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130437794839.html">Device for providing a reagent to a reaction zone of a reactor flow buffer.The reactor flow buffer and methods to minimize the radial variation of concentration at the entrance of a reagent in the reaction zone of a reactor, flow of a reaction buffer and polidispersividadeThe polymerization</a> <b>[P]</b> . 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