5-(alpha-Halobenzyl)- and 5-Benzylidene-2,2-dimethyl-1,3-oxazolidin-4-ones in Synthesis of alpha-Hydroxy Acids

Mamedov V. A.; Mamedova V. L.; Khikmatova G. Z.; Korshin D. E.; Sinyashin O. G.

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5-(alpha-Halobenzyl)- and 5-Benzylidene-2,2-dimethyl-1,3-oxazolidin-4-ones in Synthesis of alpha-Hydroxy Acids

机译：5-（α-卤苄基） - 和5-苄基-2,2-二甲基-1,3-恶唑烷-4-α-羟基酸合成

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摘要

The reactions of acid hydrolysis of 5-(alpha-halobenzyl)- and 5-benzylidene-2,2-dimethyl-1,3-oxazolidin-4-ones were studied. A possibility of the synthesis of corresponding alpha-hydroxy acids was shown.

机译：研究了5-（α-卤代苄基） - 和5-苄基-2,2-二甲基-1,3-恶唑烷-4-甲基酸水解的反应。显示了合成相应的α-羟基酸的可能性。

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来源
《Russian Journal of General Chemistry》 |2017年第12期|共9页
作者
Mamedov V. A.; Mamedova V. L.; Khikmatova G. Z.; Korshin D. E.; Sinyashin O. G.;
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作者单位

Russian Acad Sci Arbuzov Inst Organ &

Phys Chem Kazan Sci Ctr Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci Arbuzov Inst Organ &

Phys Chem Kazan Sci Ctr Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci Arbuzov Inst Organ &

Phys Chem Kazan Sci Ctr Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci Arbuzov Inst Organ &

Phys Chem Kazan Sci Ctr Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

Russian Acad Sci Arbuzov Inst Organ &

Phys Chem Kazan Sci Ctr Ul Akad Arbuzova 8 Kazan 420088 Tatarstan Russia;

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正文语种 eng
中图分类化学;
关键词
5-(halobenzyl)-2; 2-dimethyl-1; 3-oxazolidin-4-ones; 5-benzylidene-2; 2-dimethyl-1; 3-oxazolidin-4ones; 3-halo-2-hydroxy-3-arylpropionic acids; 2-hydroxy-3-arylacrylic acids; stereoselectivity;

机译：5-（卤代苄基）-2;2-二甲基-1;3-恶唑烷-4-α;5-苄基 - 2;2-二甲基-1;3-恶唑烷 - 4酮;3-卤素-2-羟基-3- 芳基丙酸;2-羟基-3-芳基丙烯酸;立体选择性;

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专利

1. 5-(alpha-Halobenzyl)- and 5-Benzylidene-2,2-dimethyl-1,3-oxazolidin-4-ones in Synthesis of alpha-Hydroxy Acids [J] . Mamedov V. A., Mamedova V. L., Khikmatova G. Z., Russian Journal of General Chemistry . 2017,第12期

机译：5-（α-卤苄基） - 和5-苄基-2,2-二甲基-1,3-恶唑烷-4-α-羟基酸合成
2. (S)-3-Dimethylamino-2-{(4S,5R)-5-[(R)-2,2-dimethyl-1,3-dioxolan-4-yl]-2,2-dimethyl-1,3-dioxolan-4-yl}-2-hydroxypropanoic acid [J] . Cowley A.R., Fleet G.W.J., Hotchkiss D.J., Acta Crystallographica Section E: Crystallographic Communications . 2008,第1期

机译：（S）-3-二甲基氨基-2 - {（4S，5R）-5 - [（R）-2,2-二甲基-1,3-二氧戊醇-4-基] -2,2-二甲基-1,3 -dioxolan-4-yl} -2-羟基丙酸
3. Reaction between 5-benzylidene-2,2-dimethyl-1,3-dioxane-4,6-dione and tert-butyl isocyanide in the presence of ethane-1,2-diol or catechol [J] . Yavari I, Zare H, Mohtat B Journal of Chemical Research. Synopses . 2007,第3期

机译：在乙烷-1,2-二醇或邻苯二酚存在下，5-亚苄基-2,2-二甲基-1,3-二恶烷-4,6-二酮与叔丁基异氰酸酯之间的反应
4. Construction of one new coordination polymers based on 5-(pyridin-4-yl)isophthalic acid acid ligands: synthesis, crystal structures and magnetism [C] . Ya-Ning Wang, Shi-Jie Li, Wen-Dong Song International Conference on Mechatronics, Robotics and Automation . 2015

机译：基于5-（吡啶-4-基）间苯二甲酸配体的一种新配位聚合物的构建：合成，晶体结构和磁
5. Synthesis, Structure and Photochemistry of Fe(III) Complexes with Tripodal Amine Chelates Containing alpha-hydroxy Acid and alpha-hydroxy Amide Groups. [D] . Vernia, Jennifer E. 2017

机译：Fe（III）与含有α-羟基酸和α-羟基酰胺基团的三脚架胺螯合物的合成，结构和光化学。
6. 5-(1H-Indol-3-ylmethylene)-4-oxo-2-thioxothiazolidin-3-yl)alkancarboxylic Acids as Antimicrobial Agents: Synthesis Biological Evaluation and Molecular Docking Studies [O] . Volodymyr Horishny, Victor Kartsev, Athina Geronikaki, 2020

机译：5-（1H-吲哚-3-基亚甲基）-4-氧代-2-硫代噻唑并恶唑烷-3-基）烷基羧酸作为抗微生物剂：合成生物学评估和分子对接研究
7. Efficient Synthesis of 5,5-(Phenylmethylene)bis(2,2-dimethyl-1,3-dioxane-4,6-dione) Derivatives in Biobased Gluconic Acid Aqueous Solution [O] . Chunhua Lin, Jianjun Yuan, Deyong Liu, 2017

机译：生物化葡萄糖酸水溶液中的5,5-（苯基甲基）双（2,2-二甲基-1,3-二恶烷-4,6-二酮）衍生物的高效合成

5-(alpha-Halobenzyl)- and 5-Benzylidene-2,2-dimethyl-1,3-oxazolidin-4-ones in Synthesis of alpha-Hydroxy Acids

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