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Preparation of tin oxide (IV) nanoparticles by a green chemistry method and investigation of its role in the removal of organic dyes in water purification

机译:用绿色化学法制物制备氧化锡(IV)纳米颗粒及其在净水中除去有机染料中的作用

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摘要

In this research, tin oxide nanoparticles (SnO2-nanoparticles) are synthesized using sol-gel method in polymeric bed and considering the principals of green chemistry. Tin chloride and gelatin were used as tin precursor and stabilizing agent, respectively. The obtained gel was calcined in different temperatures (600, 700, and 800 degrees C). Different analyses such as TG-DTA, EDX, XRD, FT-IR, TEM, and FESEM were performed to examine the prepared nanoparticles. Results of XRD, TEM, and FESEM showed the spherical SnO2-nanoparticles in a tetragonal rutile morphology with mean particle size 27 nm. The evaluation of optical attributes of SnO2 has been carried out by utilizing the UV-visible spectrophotometry. The photocatalytic activity of SnO2-nanoparticles showed efficiency about 35.9% in degradation of Eriochrome Black T (EBT).
机译:在该研究中,在聚合物床中使用溶胶 - 凝胶法合成氧化锡纳米颗粒(SnO2-纳米颗粒),并考虑到绿色化学的主体。 氯化锡和明胶分别用作锡前体和稳定剂。 将所得凝胶在不同温度(600,700和800℃)中煅烧。 进行不同的分析,例如TG-DTA,EDX,XRD,FT-IR,TEM和FESEM以检查制备的纳米颗粒。 XRD,TEM和FeSEM的结果显示,具有平均粒径27nm的四角金红石形态中的球形SnO2-纳米颗粒。 通过利用UV可见的分光光度法进行SnO2的光学属性的评价。 SnO2-纳米粒子的光催化活性显示效率约为35.9%的Eriochrome Black T(EBT)。

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