A green, efficient, and rapid procedure for the hydrogenation of nitroarenes to formanilides in water

Wang Yingying; Zhan Zhajun; Zhou Yang; Lei Min; Hu Lihong

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A green, efficient, and rapid procedure for the hydrogenation of nitroarenes to formanilides in water

机译：用于在水中氢化硝基甲烷的绿色，高效和快速的方法

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摘要

A green, efficient, and rapid procedure for the hydrogenation of nitroarenes to formanilides in Pd(TFA)(2)/HCOOH system in water is described. Under optimized conditions, the reaction of most substrates is complete within 30 min with yields of 30-93%. Furthermore, this procedure is applied successfully for the modification of natural products, such as arctigenin, vindoline, and estrone.

机译：描述了在Pd（TFA）/ HCOOH系统中氢化Nitarenes在水中氢化的绿色，有效和快速的方法。在优化的条件下，大多数底物的反应在30分钟内完成，产率为30-93％。此外，该程序成功地应用于天然产物的改性，例如芳基因素，屈糖和雌激素。

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来源
《Monatshefte fur Chemie》 |2018年第3期|共7页
作者
Wang Yingying; Zhan Zhajun; Zhou Yang; Lei Min; Hu Lihong;
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作者单位

Zhejiang Univ Technol Coll Pharmaceut Sci Hangzhou 310032 Zhejiang Peoples R China;

Zhejiang Univ Technol Coll Pharmaceut Sci Hangzhou 310032 Zhejiang Peoples R China;

Chinese Acad Sci Shanghai Inst Mat Med Shanghai Res Ctr Modernizat Tradit Chinese Med Shanghai 201203 Peoples R China;

Chinese Acad Sci Shanghai Inst Mat Med Shanghai Res Ctr Modernizat Tradit Chinese Med Shanghai 201203 Peoples R China;

Nanjing Univ Chinese Med Stake Key Lab Cultivat Base TCM Qual &

Efficacy Jiangsu Collaborat Innovat Ctr Chinese Med Resour Jiangsu Key Lab Funct Subst Chinese Med Sch Pharm Nanjing Jiangsu Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
Formanilide; Hydrogenation; Pd(TFA)(2)/HCOOH; Green chemistry;

机译：甲酰胺;氢化;Pd（TFA）（2）/ HCOOH;绿色化学;

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专利

1. A green, efficient, and rapid procedure for the hydrogenation of nitroarenes to formanilides in water [J] . Wang Yingying, Zhan Zhajun, Zhou Yang, Monatshefte fur Chemie . 2018,第3期

机译：用于在水中氢化硝基甲烷的绿色，高效和快速的方法
2. Palladium nanoparticles embedded in mesoporous carbons as efficient, green and reusable catalysts for mild hydrogenations of nitroarenes [J] . Enneiymy Mohamed, Fioux Philippe, Le Drian Claude, RSC Advances . 2020,第60期

机译：钯纳米粒子嵌入中孔碳中，作为硝基甲烷的温和氢化的高效，绿色和可重复使用的催化剂
3. Palladium nanoparticles embedded in mesoporous carbons as efficient, green and reusable catalysts for mild hydrogenations of nitroarenes [J] . Mohamed Enneiymy, Philippe Fioux, Claude Le Drian, RSC Advances . 2020,第60期

机译：钯纳米粒子嵌入中孔碳中，作为硝基甲烷的温和氢化的高效，绿色和可重复使用的催化剂
4. MCM-41 Immobilized Cobalt Tetrasulfophthalocyanine Monomer: A Green, Simple and Efficient Catalyst for the Degradative Hydrogen Peroxide Oxidation of Azo Dyes in Water [C] . Yuezhong Wen, Chensi Shen, Weiping Liu ICEC 2010;International conference on environmental catalysis . 2010

机译：MCM-41固定化钴四硫代酞菁钴单体：一种绿色，简单而高效的催化剂，用于降解水中的偶氮染料过氧化氢。
5. Design and study of catalytic activators of hydrogen peroxide promising rapid, efficient petroleum desulfurization and bleaching technologies. [D] . Hangun, Yelda. 2002

机译：过氧化氢催化活化剂的设计和研究有望实现快速，有效的石油脱硫和漂白技术。
6. Bimetallic Pd–Au/TiO2 Nanoparticles:An Efficient and Sustainable Heterogeneous Catalyst for Rapid CatalyticHydrogen Transfer Reduction of Nitroarenes [O] . Bhairi Lakshminarayana, Gedu Satyanarayana, *, 2018

机译：Pd–Au / TiO2双金属纳米颗粒：高效可持续的多相催化剂用于快速催化硝基芳烃的氢转移还原
7. Facile and green synthesis of palladium nanoparticles loaded into cyclodextrin nanofibers and their catalytic application in nitroarene hydrogenation [O] . Asli Celebioglu, Fuat Topuz, Tamer Uyar 2019

机译：钯纳米粒子的容易和绿色合成加载到环糊精纳米纤维中的催化应用及其在硝基氢化中的催化应用

A green, efficient, and rapid procedure for the hydrogenation of nitroarenes to formanilides in water

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