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The influence of parameters of disk electrode with guard electrode system and sample on permittivity error caused by equivalent electrode area calculation and its correction method

机译:磁盘电极参数与保护电极系统的影响及对等效电极区域计算引起的介电常数误差的影响及其校正方法

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摘要

To improve the accuracy in the permittivity measurement using disk electrode with guard electrode, a 3D model of this type of electrode is built in Comsol software and validated. The influence of parameters of sample and disk electrode with guard electrode system on the permittivity error caused by equivalent electrode area calculation is systematically investigated. The results reveal that the permittivity errors by means of the equivalent electrode area presented by the IEC 60250 standard are nearly always negative. From a global perspective, the area of the guarded electrode is closer to the accurate equivalent electrode area than the area provided by the IEC 60250 standard. The error decreases with increasing sample thickness and increases with increasing sample permittivity, gap width, radius of the electrode corner. If the sample is thick and the permittivity is low, the error increases significantly with increasing guarded electrode potential. The sample radius has nothing to do with the accuracy if it is slightly larger than the inside radius of the guard electrode. In the normal range, the size of shielding box, the electrode location, the deviation between the guarded electrode and the whole electrode center, the deviation between the guard electrode and the unguarded electrode, and the potential of the bolt have little effect on the accuracy. Based on the model, a permittivity correction method based on interpolation is proposed. First, the models with different parameters of electrode system and sample, measured and real values of permittivity are built. Second, the relationship among parameters of electrode system and sample is obtained. Finally, the measured permittivity can be corrected by using the relationship and the interpolation method. The accuracy in the permittivity measurement is greatly improved. Because of taking potential of guarded electrode and radius of the electrode corner into account, the error introduced by the proposed method is less than that of the existing correction methods in some situations.
机译:为了使用带保护电极的磁盘电极提高介电常数测量的准确性,在COMSOL软件中建立了这种电极的3D模型并验证。系统研究了样品和盘电极参数对由等效电极区域计算引起的介电常数误差的影响。结果表明,IEC 60250标准呈现的等效电极区域的介电常数误差几乎始终是负的。从全局角度来看,保护电极的面积比IEC 60250标准提供的区域更靠近准确的等效电极区域。误差随着样品厚度的增加而降低,随着样本介电常数,间隙宽度,电极角的半径而增加。如果样品厚,并且介电常数低,则误差随着守护电极电位的增加而显着增加。如果略大于保护电极的内半径,则样品半径与准确性无关。在正常范围内,屏蔽盒的尺寸,电极位置,保护电极和整个电极中心之间的偏差,保护电极和透明电极之间的偏差,并且螺栓的电位对准确度几乎没有影响。基于该模型,提出了一种基于插值的介电常数校正方法。首先,建立了电极系统和样本参数,测量和介电常数的实际值的模型。其次,获得电极系统和样品的参数之间的关系。最后,可以通过使用关系和插值方法来校正测量的介电常数。介电常数测量中的准确性大大提高。由于考虑到电极角的保护电极和半径的潜力,所提出的方法引入的误差小于某些情况下的现有校正方法的误差。

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