A simple and efficient synthesis of 3-(polyfluoroalkyl)-propane-1,2,3-trione 2-oximes

Filyakova Vera I.; Boltachova Nadezhda S.; Pervova Marina G.; Palysaeva Nadezhda V.; Slepukhin Pavel A.; Sheremetev Aleksei B.; Charushin Valery N.

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A simple and efficient synthesis of 3-(polyfluoroalkyl)-propane-1,2,3-trione 2-oximes

机译：3-（聚氟烷基） - 丙烷-1,2,3-Trione 2-肟的简单有效合成

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A convenient direct synthesis of 1-aryl-3-(polyfluoroalkyl)propane-1,2,3-trione 2-oximes from the corresponding lithium 3-(polyfluoroalkyl)-1,3-diketonates has been elaborated using sodium nitrite/acetic acid system under very mild conditions. The molecular structure of 4,4-difluoro-1-phenylbutane-1,2,3-trione 2-oxime has been determined by X-ray crystallography.

机译：使用亚硝酸钠/乙酸，详细阐述了来自相应锂3-（聚氟烷基）-1,3-二酮的1-芳基-3-（聚氟烷基）丙烷-1,2,3-Trione2-肟的方便合成。系统在非常温和的条件下。通过X射线晶体学确定4,4-二氟-1-苯基丁烷-1,2,3-三酮2-肟的分子结构。

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来源
《Mendeleev Communications 》 |2017年第5期| 共2页
作者
Filyakova Vera I.; Boltachova Nadezhda S.; Pervova Marina G.; Palysaeva Nadezhda V.; Slepukhin Pavel A.; Sheremetev Aleksei B.; Charushin Valery N.;
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Russian Acad Sci I Ya Postovsky Inst Organ Synth Ural Branch Ekaterinburg 620990 Russia;

Russian Acad Sci I Ya Postovsky Inst Organ Synth Ural Branch Ekaterinburg 620990 Russia;

Russian Acad Sci I Ya Postovsky Inst Organ Synth Ural Branch Ekaterinburg 620990 Russia;

Russian Acad Sci ND Zelinsky Inst Organ Chem Moscow 119991 Russia;

Russian Acad Sci I Ya Postovsky Inst Organ Synth Ural Branch Ekaterinburg 620990 Russia;

Russian Acad Sci ND Zelinsky Inst Organ Chem Moscow 119991 Russia;

Russian Acad Sci I Ya Postovsky Inst Organ Synth Ural Branch Ekaterinburg 620990 Russia;

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正文语种 eng
中图分类化学 ;
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机译：3-（聚氟烷基） - 丙烷-1,2,3-Trione 2-肟的简单有效合成
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A simple and efficient synthesis of 3-(polyfluoroalkyl)-propane-1,2,3-trione 2-oximes

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