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Synthesis and Characterization of Gold-Silver Nanoparticles in Deionized Water by Pulsed Laser Ablation (PLAL) Technique at Different Laser Parameter

机译:不同激光参数脉冲激光烧蚀(PLAL)技术在去离子水中金银纳米粒子的合成与表征

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摘要

Gold and silver nanoparticles (NPs) are physically synthesized using Q-switched neodymium-doped yttrium aluminum garnet (Nd:YAG)-pulsed laser ablation in liquid (PLAL) technique which is a rapid, simple and efficient one-step synthesis. The gold and silver colloidal solutions are separately prepared by 1064nm of pulsed laser ablation of metallic target (gold and silver) which is immersed in deionized water. Ultraviolet–visible spectroscopy (UV–Vis) analysis shows the absorption band of gold and silver NPs at ~520nm and ~400nm, respectively. The absorption spectra and color variations of gold and silver NPs at three different laser parameters (output laser energies, target distances from focal point and laser time exposures). High-resolution transmission electron microscopy shows the spherical shape of gold and silver NPs with 34nm and 33nm diameter of size, respectively, are reported. The aggregation and particle sizes of gold and silver NPs due to minimum energy (75mJ) and maximum energy (311mJ) are observed.
机译:使用Q开关的钕掺杂的钇铝石榴石(ND:YAG)在液体(PLAL)技术中进行金和银纳米粒子(NPS),其液体(PLAL)技术是一种快速,简单而有效的一步合成。通过1064nm的金属靶(金和银)的1064nm分别制备金和银胶体溶液,所述金属靶(金和银)浸入去离子水中。紫外 - 可见光谱(UV-VI)分析显示金和银NPS的吸收带,分别为520nm和〜400nm。三种不同激光参数的金和银NPS的吸收光谱和颜色变化(输出激光能量,距焦点和激光时间曝光的目标距离)。高分辨率透射电子显微镜显示出具有34nm和33nm直径的金色和银NPS的球形,分别为大小。观察到由于最小能量(75MJ)和最大能量(311MJ)的金和银NPS的聚集和粒径。

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