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首页> 外文期刊>Asian Journal of Organic Chemistry >Isocyanide‐Based Multicomponent Reactions: A Concise Approach to 2‐Amino‐3‐perfluoroalkylfurans Using Methyl Perfluoroalk‐2‐ynoates as Fluorinated Building Blocks
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Isocyanide‐Based Multicomponent Reactions: A Concise Approach to 2‐Amino‐3‐perfluoroalkylfurans Using Methyl Perfluoroalk‐2‐ynoates as Fluorinated Building Blocks

机译：基于异氰化物的多组分反应：使用甲基全氟烷-2-烃酸盐作为氟化积木的2-氨基-3-全氟烷基氧基磺脲类的简明方法

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Abstract >Synthesis of 2‐amino‐3‐perfluoroalkylfurans has been accomplished by isocyanide‐based multicomponent reactions. Using methyl perfluoroalk‐2‐ynoates as the fluorinated build blocks in combination with isocyanides and aromatic aldehydes in one‐pot at room temperature, the perfluoroalkyl‐substituted 2‐aminofurans were obtained in good to excellent yields. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 2-氨基-3-全氟烷基磺脲类的合成已经通过基于异氰化物的多组分反应来实现。 使用甲基全氟烷-2-炔酸盐作为氟化浓缩块与在室温下单罐中的异氰酸酯和芳香族醛组合，优质产率优异地获得全氟烷基取代的2-氨基呋喃。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19765/'>《Asian Journal of Organic Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2019年第5期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yedong&option=202" target="_blank" rel="nofollow">Wang Yedong;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tao Lili&option=202" target="_blank" rel="nofollow">Tao Lili;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Jie&option=202" target="_blank" rel="nofollow">Chen Jie;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=He Weimin&option=202" target="_blank" rel="nofollow">He Weimin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Deng Hongmei&option=202" target="_blank" rel="nofollow">Deng Hongmei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shao Min&option=202" target="_blank" rel="nofollow">Shao Min;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Hui&option=202" target="_blank" rel="nofollow">Zhang Hui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Cao Weiguo&option=202" target="_blank" rel="nofollow">Cao Weiguo;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry Innovative Drug Research CenterShanghai UniversityShanghai 200444 P. R. China;</p> <p>Department of Chemistry Innovative Drug Research CenterShanghai UniversityShanghai 200444 P. R. China;</p> <p>Department of Chemistry Innovative Drug Research CenterShanghai UniversityShanghai 200444 P. R. China;</p> <p>Department of Chemistry Innovative Drug Research CenterShanghai UniversityShanghai 200444 P. R. China;</p> <p>Laboratory for MicrostructuresInstrumental Analysis and Research Center of Shanghai UniversityShanghai 200444 P. R. China;</p> <p>Laboratory for MicrostructuresInstrumental Analysis and Research Center of Shanghai UniversityShanghai 200444 P. R. China;</p> <p>Laboratory for MicrostructuresInstrumental Analysis and Research Center of Shanghai UniversityShanghai 200444 P. R. China;</p> <p>Department of Chemistry Innovative Drug Research CenterShanghai UniversityShanghai 200444 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=furan&option=203" rel="nofollow">furan;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=perfluoroalkylated&option=203" rel="nofollow">perfluoroalkylated;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=isocyanide-based multicomponent reactions&option=203" rel="nofollow">isocyanide-based multicomponent reactions;</a> </p> <div class="translation"> 机译：呋喃;全氟烷基化;基于异氰化物的多组分反应; </div> </li> <li> <span class="lefttit">入库时间</span> <span>2022-08-20 01:29:24</span> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022774332.html">Isocyanide‐Based Multicomponent Reactions: A Concise Approach to 2‐Amino‐3‐perfluoroalkylfurans Using Methyl Perfluoroalk‐2‐ynoates as Fluorinated Building Blocks</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Yedong&option=202" target="_blank" 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target="_blank" rel="nofollow" class="tuijian_authcolor"> . 上海大学学报：自然科学版 </a> </span> <span> . 1997</span><span>,第S1期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_acta-laser-biology-sinica_thesis/0201254577339.html">N-(4-甲基-2-氨基苯并噻唑)α-氨基-α-(3-三氟甲基苯基)-O,O-二(2-烷氧基乙基)亚膦酸酯对小麦赤霉病原菌的抑制活性及作用机制的初步探究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄银久&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 黄银久</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘芳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘芳</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴守伟&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吴守伟</a> <span> <a href="/journal-cn-5048/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 激光生物学报 </a> </span> <span> . 2009</span><span>,第006期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_su-yan-technology_thesis/020123432780.html">对N-(2-二甲基氨基-乙基)-2-甲氧基-N-甲基-N-4-(1-甲基-1H-吲哚-3-基)-嘧啶-2-基-5-氨基-苯-1,4-二胺合成的研究</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=毛波&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 毛波</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李彦雄&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李彦雄</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=蒙发明&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,蒙发明</a> <span> <a href="/journal-cn-9404/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 苏盐科技 </a> </span> <span> . 2018</span><span>,第001期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-8470_thesis/020222147054.html">Cu(Ⅰ)催化的全氟烷基炔酸酯与2-氨基苯甲氰反应高效合成2-全氟烷基喹啉衍生物</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=韩靖&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 韩靖</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=边凌林&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,边凌林</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曹隆&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曹隆</a> <span> <a href="/conference-cn-8470/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国化学会第十二届全国氟化学会议 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020312436270.html">α-取代烃基膦酸衍生物研究之八:α-(三氟甲基取代苯氧乙酰氧基)烃基膦酸二甲酯、α-[2-氯-4-三氟甲基苯氧基苯甲酰氧基(苯甲酰氧基乙酰氧基)]烃基膦酸酯及α-氯代烃基(次)膦酸(酯)的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=黄刚良&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 黄刚良</a> <span> . 2000</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120104434849.html">内皮肽拮抗剂:N－2'－(4,5－二甲基－3－异噁唑基)氨基磺酰基－4－(2－噁唑基)1,1'联苯基－2－基甲基－N,3,3－三甲基丁酰胺和N－(4,5－二甲基－3－异噁唑基)－2'－3,3－二甲基－2－氧－1－吡咯烷基)甲基－4'－2－噁唑基)1,1'－联苯基－2－磺酰胺及其盐</a> <b>[P]</b> . <span> 中国专利： CN1244862A </span> <span> . 2000-02-16</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120104428793.html">由N－全氟烷基甲基亚氨基代芳酰氯化合物制备2－芳基－5－全氟烷基吡咯化合物的方法</a> <b>[P]</b> . <span> 中国专利： CN1230539A </span> <span> . 1999-10-06</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130409289636.html">Pyridine-based isocyanides as novel reagents for multicomponent reactions.</a> <b>[P]</b> . <span> 外国专利： <!-- --> NL2015814B1 </span> <span> . 2017-06-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：吡啶基异氰酸酯是用于多组分反应的新型试剂。 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130437785777.html">Process for preparing 4 - methyl - 3 - 4 - (3-pyridinyl) - 2 - pirimidinil - amino - N - substituted by reaction between the corresponding Ester and an Amine in the presence of base.</a> <b>[P]</b> . <span> 外国专利： <!-- --> CL2006001402A1 </span> <span> . 2006-09-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：制备4-甲基-3-[[[4-（3-吡啶基）-2-吡啶胺]-氨基] -N-的方法，该方法是在碱存在下通过相应的酯和胺之间的反应进行取代的。 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130482786009.html">p-Chloro-phenoxy-acetic acid salt of 6-amino-2-methyl heptanol - used as cough remedy and obtd by reaction of the acid with the base</a> <b>[P]</b> . <span> 外国专利： <!-- 德国专利： --> DE2504546A1 </span> <span> . 1976-08-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：6-氨基-2-甲基庚醇的对氯苯氧基乙酸盐-用作止咳药，通过酸与碱的反应而被消除 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704022774332','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" 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