Large Crystals Synthesis of Siliceous Layered Zeolitic PLS‐1 and CDS‐1 Zeolite by Dry Gel Conversion Method

机译：通过干凝胶转化方法大晶体合成硅质分层沸石PLS-1和Cds-1沸石

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Abstract > The large crystal of siliceous zeolitic layered PLS‐1, which is a precursor of CDS‐1 zeolite with CDO ‐type topology, can be successfully prepared by dry‐gel conversion (DGC) method from a dry‐gel containing layered silicate H‐kanemite and tetramethylammonium hydroxide (TMAOH) as an organic structure‐directing agent (OSDA), and it allows transform to CDS‐1 zeolite by calcination with retaining its large crystal particle. Characterizations of the obtained CDS‐1 zeolite reveal the different morphology compared by conventional methods. Its particle is found to be aggregated by an enlarged thickness of layered crystals reflecting a zeolitic precursor of PLS‐1. Gradual increases of nitrogen adsorption at around middle pressure and FE‐SEM measurements strongly indicate that the obtained particles have many steps and aperture like card‐house assembly of layered PLS‐1 large crystals. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >硅质沸石分层PLS-1的大晶体，这是Cds-1的前兆具有<B> CDO </ B> -Type拓扑的沸石可以通过干凝胶转化（DGC）方法从含有层状硅酸盐H- kahemite和四甲基氢氧化铵（TMAOH）的干凝胶作为有机结构引导的干凝胶转化（DGC）方法成功制备代理（OSDA），它允许通过煅烧转换为Cds-1沸石，通过保持其大晶粒。所得Cds-1沸石的特征揭示了通过常规方法比较的不同形态。发现其颗粒通过反射PLS-1的沸石前体的层状晶体的扩大厚度聚集。在中压和Fe-SEM测量周围的氮吸附的逐渐增加强烈表示所获得的颗粒具有许多步骤和孔径，如层状PLS-1大晶体的卡房组件。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18164/'>《Crystal Research and Technology: Journal of Experimental and Industrial Crystallography》</a> <b style="margin: 0 2px;">|</b><span>2018年第7期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Banno Shohei&option=202" target="_blank" rel="nofollow">Banno Shohei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Komura Kenichi&option=202" target="_blank" rel="nofollow">Komura Kenichi;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Materials Science and TechnologyGifu UniversityGifu 501–1193 Japan;</p> <p>Department of Materials Science and TechnologyGifu UniversityGifu 501–1193 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/160.html" title="晶体学">晶体学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=CDO topology&option=203" rel="nofollow">CDO topology;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=CDS‐1&option=203" rel="nofollow">CDS‐1;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=dry gel conversion&option=203" rel="nofollow">dry gel conversion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=H‐kanemite&option=203" rel="nofollow">H‐kanemite;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=PLS‐1&option=203" rel="nofollow">PLS‐1;</a> </p> <div class="translation"> 机译：CDO拓扑;CDS-1;干凝胶转换;H-KANEMITE;PLS-1; 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Chen Tuxing</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈土兴&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,陈土兴</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hu Jingbo&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Hu Jingbo</a> <span> <a href="/conference-cn-40601/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国工程建设标准化协会防水防护专业委员会换届年会暨2016工程建设新型防水防护学术技术交流会 </a> <span> <span> . 2016</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314127318.html">全硅沸石吸/脱附性质的研究及四氢呋喃导向沸石的合成</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=钱斌&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 钱斌</a> <span> . 2001</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120107092765.html">用于晶体生长、仅诱导从硅沸石-1或沸石β晶种表面的二次生长的合成凝胶</a> <b>[P]</b> . <span> 中国专利： CN104583220A </span> <span> . 2015-04-29</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120110357.html">使用大晶体沸石催化剂的烃转化方法</a> <b>[P]</b> . <span> 中国专利： CN1104402C </span> <span> . 2003.04.02</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130439102982.html">Production of enclosed zeolite layers for use in e.g. catalysis or separation membranes, comprises first seed crystallization on carrier followed by further crystallization using different synthesis solution or gel</a> <b>[P]</b> . <span> 外国专利：  DE10304322A1 </span> <span> . 2004-11-18</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：封闭的沸石层的生产用于例如催化或分离膜，包括首先在载体上进行晶种结晶，然后使用不同的合成溶液或凝胶进一步晶化 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130416199321.html">crystal to induce only secondary growth from the surface of the silicalite-1 or more of zeolite beta of the seed crystal growth synthesis gel</a> <b>[P]</b> . <span> 外国专利：  JP2015526366A </span> <span> . 2015-09-10</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：晶体仅诱导硅晶1表面或更多种晶生长合成凝胶的β沸石表面的二次生长 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130433592250.html">CRYSTALLINE LAYERED SILICATE BY SOLID PHASE REACTION METHOD IN STEAM ATMOSPHERE AND RAPID SYNTHESIS METHOD OF ZEOLITE</a> <b>[P]</b> . <span> 外国专利：  JP2007332004A </span> <span> . 2007-12-27</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> 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