Chemical Vapor Deposition of 2D Vanadium Disulfide and Diselenide and Raman Characterization of the Phase Transitions

Hossain Mongur; Wu Juanxia; Wen Wen; Liu Haining; Wang Xinsheng; Xie Liming

摘要

Abstract > 2D metallic vanadium dichalcogenides (VX <sub>2</sub> ) have renewed interest due to their unique physical properties and potential applications as high‐performance functional nanomaterials. Herein, the synthesis and phase transitions of 2D metallic VX <sub>2</sub> are investigated. The synthesis is done by chemical vapor deposition using hexagonal boron nitride and mica as substrates. High‐quality VX <sub>2</sub> flakes with sub‐10 nm thickness are obtained and characterized by transmission electron microscopy. Temperature‐dependent Raman characterization between 330 and 5 K is conducted and remarkable changes of Raman modes at around 150 K for VS <sub>2</sub> flakes and 110 K for VSe <sub>2</sub> flakes are revealed, indicating charge density wave phase transitions. Temperature‐dependent electrical measurements have also supported the phase transitions observed in Raman characterization. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 2D金属钒二甲硅藻（Vx <sub> 2 </ sub> ）由于其独特的物理性质和潜在应用而重新兴趣，作为高性能官能纳米材料。在此，2D金属Vx的合成和相变 <sub> 2 </ sub> 调查。通过使用六边形氮化硼和云母作为基材来通过化学气相沉积来完成合成。高质量的vx <sub> 2 </ sub> 通过透射电子显微镜获得和表征具有亚10 NM厚度的薄片。在330和5 k之间的温度依赖拉曼表征在150 k左右的拉曼模式的变化和VS的显着变化 <sub> 2 </ sub> 薄片和110 k为VSE <sub> 2 </ sub> 显示薄片，指示电荷密度波相转变。温度依赖性电测量也支持拉曼表征中观察到的相变。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2018年第16期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hossain Mongur&option=202" target="_blank" rel="nofollow">Hossain Mongur;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Juanxia&option=202" target="_blank" rel="nofollow">Wu Juanxia;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wen Wen&option=202" target="_blank" rel="nofollow">Wen Wen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Haining&option=202" target="_blank" rel="nofollow">Liu Haining;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Xinsheng&option=202" target="_blank" rel="nofollow">Wang Xinsheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Xie Liming&option=202" target="_blank" rel="nofollow">Xie Liming;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> <p>CAS Key Laboratory of Standardization and Measurement for NanotechnologyNational Center for Nanoscience and TechnologyBeijing 100190 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=charge density wave&option=203" rel="nofollow">charge density wave;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chemical vapor deposition&option=203" rel="nofollow">chemical vapor deposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrical measurement&option=203" rel="nofollow">electrical measurement;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=temperature‐dependent Raman spectroscopy&option=203" rel="nofollow">temperature‐dependent Raman spectroscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=vanadium dichalcogenide&option=203" rel="nofollow">vanadium dichalcogenide;</a> </p> <div class="translation"> 机译：电荷密度波;化学气相沉积;电气测量;温度依赖拉曼光谱;钒二甲基化物; 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