Bistetracene Thin Film Polymorphic Control to Unravel the Effect of Molecular Packing on Charge Transport

Burnett Edmund K.; Ly Jack; Niazi Muhammad R.; Zhang Lei; McCuskey Samantha R.; Amassian Aram; Smilgies Detlef‐M.; Mannsfeld Stefan C. B.; Briseno Alejandro L.

摘要

Abstract >Polymorphism, the ability for a given material to adopt multiple crystalline packing states, is a powerful approach for investigating how changes in molecular packing influence charge transport within organic semiconductors. In this study, a new “thin film” polymorph of the high‐performance, p‐type small molecule N‐octyldiisopropylsilyl acetylene bistetracene (BT) is isolated and characterized. Structural changes in the BT films are monitored using static and in situ grazing‐incidence X‐ray diffraction. The diffraction data, combined with simulation and crystallographic refinement calculations, show the molecular packing of the “thin film” polymorph transforms from a slipped 1D π‐stacking motif to a highly oriented and crystalline film upon solvent vapor annealing with a 2D brick‐layer π‐stacking arrangement, similar to the so‐called “bulk” structure observed in single crystals. Charge transport is characterized as a function of vapor annealing, grain orientation, and temperature. Demonstrating that mobility increases by three orders of magnitude upon solvent vapor annealing and displays a differing temperature‐dependent mobility behavior. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> 多态性，采用多种晶体包装状态的给定材料的能力是一种强大的方法，用于研究分子包装的变化如何影响有机半导体内的电荷输送。在该研究中，分离出并表征了一种新的“薄膜”高性能，p型小分子N-辛基二异丙基甲硅烷基乙炔双丙烯（BT）。使用静态和原位放射性X射线衍射监测BT膜的结构变化。结合模拟和晶体化细化计算的衍射数据显示，在溶剂蒸汽退火与2D砖层π上的溶剂蒸汽退火上，将“薄膜”多晶型物的分子包装从滑动的1Dπ堆叠基序转换为高度取向和结晶膜。 - 类似于在单晶中观察到的所谓的“散装”结构。电荷传输的特征在于蒸汽退火，晶粒取向和温度的函数。展示迁移率在溶剂蒸汽退火时增加了三个级的增加，并显示出不同的温度依赖性迁移行为。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Burnett Edmund K.&option=202" target="_blank" rel="nofollow">Burnett Edmund K.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ly Jack&option=202" target="_blank" rel="nofollow">Ly Jack;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Niazi Muhammad R.&option=202" target="_blank" rel="nofollow">Niazi Muhammad R.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Lei&option=202" target="_blank" rel="nofollow">Zhang Lei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=McCuskey Samantha R.&option=202" target="_blank" rel="nofollow">McCuskey Samantha R.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Amassian Aram&option=202" target="_blank" rel="nofollow">Amassian Aram;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Smilgies Detlef‐M.&option=202" target="_blank" rel="nofollow">Smilgies Detlef‐M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mannsfeld Stefan C. B.&option=202" target="_blank" rel="nofollow">Mannsfeld Stefan C. B.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Briseno Alejandro L.&option=202" target="_blank" rel="nofollow">Briseno Alejandro L.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Polymer Science and EngineeringUniversity of Massachusetts AmherstAmherst MA 01003 USA;</p> <p>Department of Polymer Science and EngineeringUniversity of Massachusetts AmherstAmherst MA 01003 USA;</p> <p>Physical Science and Engineering DivisionKing Abdullah University of Science and Technology (KAUST)Thuwal 23955‐6900 Saudi Arabia;</p> <p>Department of Polymer Science and EngineeringUniversity of Massachusetts AmherstAmherst MA 01003 USA;</p> <p>Department of Polymer Science and EngineeringUniversity of Massachusetts AmherstAmherst MA 01003 USA;</p> <p>Physical Science and Engineering DivisionKing Abdullah University of Science and Technology (KAUST)Thuwal 23955‐6900 Saudi Arabia;</p> <p>Cornell High Energy Synchrotron SourceCornell UniversityIthaca NY 14853 USA;</p> <p>Center for Advanced Electronics DresdenDresden University of Technology01062 Dresden Germany;</p> <p>Department of Polymer Science and EngineeringUniversity of Massachusetts AmherstAmherst MA 01003 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=bistetracene&option=203" rel="nofollow">bistetracene;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=organic semiconductors&option=203" rel="nofollow">organic semiconductors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polymorphism&option=203" rel="nofollow">polymorphism;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=solvent vapor annealing&option=203" rel="nofollow">solvent vapor annealing;</a> </p> <div class="translation"> 机译：Bistetracene;有机半导体;多态性;溶剂蒸汽退火; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434372.html">Bistetracene Thin Film Polymorphic Control to Unravel the Effect of Molecular Packing on 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=亢永珍&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,亢永珍</a> <span> <a href="/conference-cn-59027/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第一届全国化学工程与生物化工年会 </a> <span> <span> . 2004</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313593060.html">取代模式对基于有机硼化合物的联苯、二苯乙炔和二苯乙烯的分子内电荷转移发光性能的影响</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=晏祎峤&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 晏祎峤</a> <span> . 2014</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061202702912.html">一种氰基苯乙烯类超分子凝胶薄膜、制备方法及其在检测空气中二氧化碳浓度的应用</a> <b>[P]</b> . <span> 中国专利： CN105820813B </span> <span> . 2018.01.02</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120108324264.html">一种氰基苯乙烯类超分子凝胶薄膜、制备方法及其在检测空气中二氧化碳浓度的应用</a> <b>[P]</b> . <span> 中国专利： CN105820813A </span> <span> . 2016-08-03</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130428962031.html">METHOD OF CONTROLLING MOLECULAR ORIENTATION DIRECTION OF CHARGE-TRANSPORTING AMORPHOUS THIN FILM, AND METHOD OF MANUFACTURING CHARGE-TRANSPORTING AMORPHOUS THIN FILM</a> <b>[P]</b> . <span> 外国专利：  JP2010212112A </span> <span> . 2010-09-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：电荷输送非晶薄膜的分子取向方向的控制方法及电荷输送非晶薄膜的制造方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130421132233.html">A charge transport material for the low molecular coating-type organic electroluminescent device, an organic electroluminescence element composition, the organic electroluminescent device and an organic thin film electroluminescence device</a> <b>[P]</b> . <span> 外国专利：  JP5167747B2 </span> <span> . 2013-03-21</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于低分子涂层型有机电致发光器件的电荷传输材料，有机电致发光元件组合物，有机电致发光器件和有机薄膜电致发光器件 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130418465712.html">It does not show the control manner of numerator orientation direction of the electric charge transportability amorphous thin film, or the production mannered null clear melting point</a> <b>[P]</b> . <span> 外国专利：  JP5408474B2 </span> <span> . 2014-02-05</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：没有示出电荷输送性非晶质薄膜的分子取向方向的控制方式，或者未说明的制造方法的零熔点。 </span> </p> 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