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Influence of cleaning methods on the bond strength of resin cement to saliva-contaminated lithium disilicate ceramic

机译:清洁方法对树脂水泥对唾液污染锂静止陶瓷粘接强度的影响

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ObjectivesThe aim of the present study was to examine the influence of different cleaning methods on the bond strength of resin cement to saliva-contaminated lithium disilicate ceramic.Materials and methodsLithium disilicate ceramic specimens (n=8/group) were etched with 5% hydrofluoric acid (HF) to comprise the control group. After or before saliva contamination, specimens were cleaned with one of five methods: rinsing with water-spray (WS), K etchant GEL (PA), Ivoclean (IC), AD Gel (ADG), or application of a silane coupling agent before immersion in saliva (SCA). Stainless steel rods were bonded to the ceramic with resin cement. The tensile bond strength was measured after 24 h (TC0) and after thermal cycling at 4-60 degrees C (TC20000). Specimen surfaces were also evaluated using X-ray photoelectron spectroscopy. Data were statistically analyzed using two-way ANOVA and Tukey tests (alpha=0.05).ResultsBoth the cleaning method (p=0.0001) and storage condition (p=0.0001) significantly affected the bond strength results. Before or after TCs, no significant differences in bond strength were observed between the control group and the other cleaning groups except for the WS group, which had a significantly lower bond strength than did the PA, IC, ADG, or SCA groups (p<0.05). The level of nitrogen in the ADG group was almost equal to that in the control group.ConclusionsWS cleaning did not restore the bond strength of resin cement to saliva-contaminated lithium disilicate ceramic etched with HF, while PA, IC, ADG, and SCA all benefited.Clinical relevanceLithium disilicate ceramic restorations etched with HF should to be cleaned with ADG after saliva contamination.
机译:本研究的客观目的是检查不同清洁方法对唾液污染锂静止陶瓷的树脂水泥的键合强度的影响。用5%氢氟酸蚀刻静止硫酸锂硫酸锂锂硫酸锂硫酸锂(n = 8 /组) (HF)包含对照组。在唾液污染物污染之后,用五种方法之一清洗样品:用水喷雾(WS),K蚀刻剂凝胶(PA),IVOCLEAN(IC),ADG(ADG),或施加硅烷偶联剂之前的漂洗浸入唾液(SCA)。用树脂水泥将不锈钢棒粘合到陶瓷中。在24小时(TC0)之后测量拉伸粘合强度,在4-60℃(TC20000)的热循环后测量。还使用X射线光电子能谱评估样品表面。使用双向ANOVA和Tukey测试(alpha = 0.05)进行统计分析数据在TCS之前或之后,除了WS组外,对照组和其他清洁组之间没有观察到粘合强度的显着差异,其具有比PA,IC,ADG或SCA组的显着降低的粘合强度(P < 0.05)。 ADG组中的氮水平几乎等于对照组中的水平。结论WS清洁并未将树脂水泥的粘合强度恢复为唾液污染的锂静止陶瓷蚀刻HF,而PA,IC,ADG和SCA全部受益。用HF蚀刻的临床相关性静止陶瓷修复物应在唾液污染后用ADG清洁。

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