Behavior of a Metal Organic Framework Thin‐Film at Elevated Temperature and Pressure as Studied with an Autoclave‐Inserted Atomic Force Microscope

机译：用高压釜插入原子力显微镜研究的升高温度和压力下的金属有机框架薄膜的行为

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Abstract > Bridging the gap in studying surface reactions, processes, and morphology and measuring at (catalytic) relevant conditions is crucial for our understanding of the working principles of porous crystalline materials. Scanning tunneling microscopy is limited because of the required conductivity of the sample, whereas atomic force microscopy (AFM) is often challenging in use owing to the physical mechanism underlying the technique. Herein, we report a tailor‐made autoclave‐inserted AFM, able to measure at ～20?bar and ～110?°C. First, we show the ability to obtain nanometer resolution on well‐defined test samples at before‐mentioned conditions. Second, to demonstrate the possibilities of analyzing morphological evolutions at elevated temperatures and pressures, we use this setup to measure the stability of a surface‐anchored metal‐organic framework (SURMOF) in‐situ at pressures of 1–20?bar in the temperature range between 20 and 60?°C. It was found that the showcase HKUST‐1 material has a good physical stability, as it is hardly damaged from exposure to pressures up to 20?bar. However, its thermal stability is weaker, as exposure to elevated T damaged the material by influencing the interaction between organic linker and metal cluster. In‐situ measurements at elevated T also showed an increased mobility of the material when working at such conditions. Combining the strength of AFM at elevated T and p with ex‐situ AFM and spectroscopic measurements on this MOF showcases an example of how porous materials can be studied at (industrially) relevant conditions using the autoclave‐inserted AFM. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >桥接研究表面反应，过程和形态学的差距和（催化）相关的差距条件对于我们对多孔晶体材料的工作原理的理解至关重要。扫描隧穿显微镜由于样品所需的导电性而受到限制，而原子力显微镜（AFM）由于技术的物理机制而在使用中经常具有挑战性。在此，我们报告了一种量身定制的高压釜插入的AFM，能够测量〜20？棒和〜110？℃。首先，我们展示了在预先提及的条件下获得纳米分辨率的纳米分辨率。其次，为了证明在高温和压力下分析形态演进的可能性，我们使用该设置测量在温度下1-20？棒的压力下的表面锚定金属 - 有机框架（SURMOF）的稳定性范围在20到60°C之间。发现展示HKUST-1材料具有良好的物理稳定性，因为它几乎不会因暴露而损坏到高达20？棒的压力。然而，其热稳定性较弱，因为暴露于升高的 T </ i>通过影响有机接头和金属簇之间的相互作用而损坏了材料。在升高的 T </ i>的原位测量还显示在在这种条件下工作时材料的迁移率增加。将AFM的强度与在该MOF上的exi-sieS aFM和 P </ i>在升高的 p </ i>上结合，展示了如何在（工业上）相关的多孔材料的示例使用高压釜插入AFM的条件。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16300/'>《Chemphyschem: A European journal of chemical physics and physical chemistry》</a> <b style="margin: 0 2px;">|</b><span>2018年第18期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Brand Rogier P.&option=202" target="_blank" rel="nofollow">Brand Rogier P.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mandemaker Laurens D. B.&option=202" target="_blank" rel="nofollow">Mandemaker Laurens D. B.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Delen Guusje&option=202" target="_blank" rel="nofollow">Delen Guusje;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rijnveld Niek&option=202" target="_blank" rel="nofollow">Rijnveld Niek;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Weckhuysen Bert M.&option=202" target="_blank" rel="nofollow">Weckhuysen Bert M.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Debye Institute for Nanomaterials ScienceUtrecht UniversityUniversiteitsweg 99 3584 CG Utrecht The Netherlands;</p> <p>Debye Institute for Nanomaterials ScienceUtrecht UniversityUniversiteitsweg 99 3584 CG Utrecht The Netherlands;</p> <p>Debye Institute for Nanomaterials ScienceUtrecht UniversityUniversiteitsweg 99 3584 CG Utrecht The Netherlands;</p> <p>Optics 11De Boelelaan 1081 1081 HV Amsterdam The Netherlands;</p> <p>Debye Institute for Nanomaterials ScienceUtrecht UniversityUniversiteitsweg 99 3584 CG Utrecht The Netherlands;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=atomic force microscopy&option=203" rel="nofollow">atomic force microscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=autoclave measurements&option=203" rel="nofollow">autoclave measurements;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=catalyst stability&option=203" rel="nofollow">catalyst stability;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal-organic frameworks&option=203" rel="nofollow">metal-organic frameworks;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=scanning probe microscopy&option=203" rel="nofollow">scanning probe microscopy;</a> </p> <div class="translation"> 机译：原子力显微镜;高压灭菌测量;催化剂稳定性;金属有机框架;扫描探针显微镜; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022115943.html">Behavior of a Metal Organic Framework Thin‐Film at Elevated Temperature and Pressure as Studied with an Autoclave‐Inserted Atomic Force Microscope</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Brand Rogier P.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Brand Rogier P.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mandemaker Laurens D. 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