Templateless Electropolymerization for Controlled Growth of Polymeric Nanotubes on Micropatterned Surfaces

Bombera Radoslaw; Ramos?Chagas Gabriela; Valsesia Andrea; Colpo Pascal; Guittard Frédéric; Darmanin Thierry

摘要

Abstract >Controlling the growth of nanostructures on surfaces is fundamental to develop new materials for various fields of applications such as sensing or biomedical applications. Here, we study for the first time the influence of micropatterned substrates on the growth of nanotubes using a templateless electropolymerization approach. The influence of both the nature of the monomer and the deposition charge used in the polymerization process is assessed along with geometric parameters of the microstructured surfaces composed of bidimensionally distributed squared micropillars. First, we show that the formation of nanotubes is always favored at the basis of the microfeatures rather than on their top surface. As a consequence, it is preferable to avoid using monomers which lead to mono‐directional (1D) nanotube growth which would be only generated at the basis of the micropillars. By contrast, monomers leading to extremely short nanotubes (nanocups) are preferred. In addition, we hereby demonstrate that the surface coverage with the nanotubes is highly dependent on the geometric parameters of micropatterned substrates. Indeed, the growth of the nanostructures over the micropillars requires a significant energy and thus micropillars of lower height give optimal results. We demonstrate that it is possible to obtain a complete coverage of the microstructured substrate at even very low deposition charge applied during the electropolymerization step. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >控制表面上的纳米结构的生长是开发用于各种应用领域的新材料，例如感测或生物医学应用。在这里，我们首次学习使用TemplaTeless电池化方法对微型解放基板对纳米管生长的影响。单体性质的影响和聚合过程中使用的沉积电荷的影响以及由由偏压分布的平方微米组成的微结构化表面的几何参数。首先，我们表明纳米管的形成总是基于微泡而不是在其顶表面上受到青睐。结果，优选避免使用导致单向（1D）纳米管生长的单体，这将仅基于微米产生。相反，优选导致极短纳米管（纳米载体）的单体。此外，我们在此表明，具有纳米管的表面覆盖率高度依赖于微型解放基板的几何参数。实际上，纳米结构对微米的生长需要显着的能量，因此较低高度的微米提供最佳结果。我们证明，在电聚合步骤期间施加的甚至非常低的沉积电荷，可以获得微结构化基板的完全覆盖。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16168/'>《ChemNanoMat》</a> <b style="margin: 0 2px;">|</b><span>2019年第9期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Bombera Radoslaw&option=202" target="_blank" rel="nofollow">Bombera Radoslaw;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ramos?Chagas Gabriela&option=202" target="_blank" rel="nofollow">Ramos?Chagas Gabriela;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Valsesia Andrea&option=202" target="_blank" rel="nofollow">Valsesia Andrea;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Colpo Pascal&option=202" target="_blank" rel="nofollow">Colpo Pascal;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guittard Frédéric&option=202" target="_blank" rel="nofollow">Guittard Frédéric;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Darmanin Thierry&option=202" target="_blank" rel="nofollow">Darmanin Thierry;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>European CommissionDG Joint Research Centre TP125Via Fermi 21027 Ispra Italy;</p> <p>Université C?te d'Azur NICE Lab06100 Nice France;</p> <p>European CommissionDG Joint Research Centre TP125Via Fermi 21027 Ispra Italy;</p> <p>European CommissionDG Joint Research Centre TP125Via Fermi 21027 Ispra Italy;</p> <p>Université C?te d'Azur NICE Lab06100 Nice France;</p> <p>Université C?te d'Azur NICE Lab06100 Nice France;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1676.html" title="工程材料学">工程材料学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nanotubes&option=203" rel="nofollow">Nanotubes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Photolithography&option=203" rel="nofollow">Photolithography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Conducting polymers&option=203" rel="nofollow">Conducting polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wettability&option=203" rel="nofollow">Wettability;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Electropolymerization&option=203" rel="nofollow">Electropolymerization;</a> </p> <div class="translation"> 机译：纳米管;光刻;导电聚合物;润湿性;电聚; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022089116.html">Templateless Electropolymerization for Controlled Growth of Polymeric Nanotubes on Micropatterned Surfaces</a> 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initial;text-overflow: initial;overflow: initial;"> <span>机译：功能性双相导电聚合物聚吡咯/聚咔唑/聚噻吩（CP / polyPyr / polyCbz / PolyTh）-碳纳米管（CNT）复合材料的控制形态和组成的复合材料“侧壁生长”-侧壁与端部选择性PolyTh沉积 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130424743826.html">A "Growth from surface" Methodology for the Fabrication of Functional Dual Phase Conducting Polymer polypyrrole/polycarbazole/Polythiophene (CP/polyPyr/polyCbz/PolyTh)-Carbon Nanotube (CNT) Composites of Controlled Morphology and Composition - Sidewall versus End-Selective PolyTh Deposition</a> <b>[P]</b> . <span> 外国专利：  WO2011135560A1 </span> <span> . 2011-11-03</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：功能性双相导电聚合物聚吡咯/聚咔唑/聚噻吩（CP / polyPyr / polyCbz / PolyTh）-碳纳米管（CNT）复合材料的控制形态和组成的“从表面生长”方法-侧壁与端部选择性聚苯乙烯沉积 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" 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