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Silver Thiolate Nano‐sized Molecular Clusters and Their Supramolecular Covalent Frameworks: An Approach Toward Pre‐templated Synthesis

机译：银硫醇酸盐纳米尺寸分子簇及其超分子共价框架：预先模板合成的方法

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Abstract > A series of seven new complexes including silver‐thiolate molecular clusters and their covalent supramolecular frameworks have been assembled from the silver carbide precursor Ag <sub>2</sub> C <sub>2</sub> using a C <sub>2</sub> 2? pre‐templated approach. Herein, two prototype clusters Ag <sub>14</sub> (SR) <sub>6</sub> and CO <sub>3</sub> @Ag <sub> m </sub> (SR) <sub>10</sub> (R=isopropyl, cyclohexyl or tert ‐butyl; m= 18 or 20) are employed to construct cluster‐based metal–organic frameworks of different dimensions. In particular, both new ellipsoidal tetradecanuclear molecular cluster compounds, namely, Ag <sub>14</sub> (S‐ i Pr) <sub>6</sub> (CO <sub>2</sub> CF <sub>3</sub> ) <sub>8</sub> ?(DMSO) <sub>6</sub> (two polymorphic forms 1 , 2 ) and [Ag <sub>14</sub> (S‐Cy) <sub>6</sub> (CO <sub>2</sub> CF <sub>3</sub> ) <sub>8</sub> (DMSO) <sub>4</sub> ]?(DMSO) <sub>3</sub> ( 3 ), and a cluster‐based metal–organic framework {Ag <sub>3</sub> [Ag <sub>14</sub> (S‐ i Pr) <sub>6</sub> (CO <sub>2</sub> CF <sub>3</sub> ) <sub>11</sub> (H <sub>2</sub> O) <sub>3</sub> CH <sub>3</sub> OH]?(H <sub>2</sub> O) <sub>2.5</sub> } <sub> n </sub> ( 4 ) have been isolated and structurally characterized. Furthermore, increased acidity of the reaction mixture afforded three carboxylate‐templated cluster based frameworks: a chain‐like compound {[HN(CH <sub>3</sub> ) <sub>2</sub> CO]?[CO <sub>3</sub> @Ag <sub>18</sub> (S‐ t Bu) <sub>10</sub> (NO <sub>3</sub> ) <sub>7</sub> (DMF) <sub>4</sub> ]?DMF} <sub> n </sub> ( 5 ), as well as two layer‐type compounds, namely, {Ag[CO <sub>3</sub> @Ag <sub>20</sub> (S‐ i Pr) <sub>10</sub> (CO <sub>2</sub> CF <sub>3</sub> ) <sub>9</sub> (CO <sub>2</sub> HCF <sub>3</sub> )(CH <sub>3</sub> OH) <sub>2</sub> ]} <sub> n </sub> ( 6 ) and {Ag <sub>2</sub> [CO <sub>3</sub> @Ag <sub>20</sub> (S‐Cy) <sub>10</sub> (CO <sub>2</sub> CF <sub>3</sub> ) <sub>10</sub> (CO <sub>2</sub> HCF <sub>3</sub> ) <sub>2</sub> (H <sub>2</sub> O) <sub>2</sub> ]?(H <sub>2</sub> O) <sub>3</sub> ?(CH <sub>3</sub> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >一个系列在包括银硫醇硫醇酸盐分子簇的七个新络合物中，使用C <SUB> 2（使用C <SUB> 2 </ sub>组装银碳化物前体蛋白和它们的共价超分子框架。子> 2？</ sup>预模板化方法。这里，两个原型簇Ag <sub> 14 </ sub>（SR）<sub> 6 </ sub>和Co <sub> 3 </ sum> @Ag <sub> m </亚>（SR）<sub> 10 </ sub>（R =异丙基，环己基或 TERT </ I> - 丁基; M = </ I> 18或20）被用于构建聚类 - 基于基于金属 - 有机框架的不同尺寸。特别地，新的椭圆虫四核核簇化合物，即Ag <sub> 14 </ sub>（S- i </ i> Pr）<sub> 6 </ sub>（CO <sub> 2 < / sub> cf <sub> 3 </ sub>）<sub> 8 </ sub>？（dmso）<sub> 6 </ sub>（两种多晶型 1 </ b>， 2 </ b>）和[ag <sub> 14 </ sub>（s-cy）<sub> 6 </ sub>（co <sub> 2 </ sub> cf <sub> 3 </ sub>）<亚> 8 </ sub>（DMSO）<亚> 4 </ sub>]？（DMSO）<亚> 3 </ sub>（ 3 </ b>），以及基于簇的金属有机物框架{ag <sub> 3 </ sub> [ag <sub> 14 </ sub>（s- i </ i> pr）<sub> 6 </ sub>（co <sub> 2 </子> CF <sub> 3 </ sub>）<sub> 11 </ sub>（h <sub> 2 </ sub> o）<sub> 3 </ sub> ch <sub> 3 </ sub>哦]？（H <sub> 2 </ sub> O）<sub> 2.5 </ sub>} <sub> n </ i> </ sub>（ 4 </ b>）孤立和结构性地表征。此外，增加了反应混合物的酸度，得到了三种羧酸酯模板基簇的框架：链状化合物（[HN（CH <sub> 3 </ sub>）<sub> 2 </ sub> co]？[co <子> 3 </ sub> @Ag <sub> 18 </ sub>（s- t </ i> bu）<sub> 10 </ sub>（no <sub> 3 </ sub>）< Sub> 7 </ sub>（dmf）<sub> 4 </ sub>]？dmf} <sub> n </ i> </ sub>（ 5 </ b>）作为两层型化合物，即，{Ag [Co <sub> 3 </ sub> @Ag <sub> 20 </ sub>（s- i </ i> pr）<sub> 10 </子>（CO <sub> 2 </ sub> cf <sub> 3 </ sub>）<sub> 9 </ sub>（co <sub> 2 </ sub> hcf <sub> 3 </ sub>）（CH <sub> 3 </ sub> OH）<sub> 2 </ sub>]} <sub> n </ i> </ sub>（ 6 </ b>）和{AG <sub> 2 </ sub> [co <sub> 3 </ sub> @ag <sub> 20 </ sub>（s-cy）<sub> 10 </ sub>（co <sub> 2 </ sub > Cf <sub> 3 </ sub>）<sub> 10 </ sub>（co <sub> 2 </ sub> hcf <sub> 3 </ sub>）<sub> 2 </ sub>（h <子> 2 </ sub> O）<sub> 2 </ sub>]？（h <sub> 2 </ sub> o）<sub> 3 </ sub>？（ch <sub> 3 </ sub> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16161/'>《Chemistry, an Asian journal》</a> <b style="margin: 0 2px;">|</b><span>2017年第20期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Zi‐Yi&option=202" target="_blank" rel="nofollow">Chen Zi‐Yi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tam Dennis Y. S.&option=202" target="_blank" rel="nofollow">Tam Dennis Y. S.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Leon Li‐Min&option=202" target="_blank" rel="nofollow">Zhang Leon Li‐Min;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mak Thomas C. W.&option=202" target="_blank" rel="nofollow">Mak Thomas C. W.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Chemistry and Center of Novel Functional MoleculesThe Chinese University of Hong KongShatin New Territories Hong Kong SAR People's Republic of China;</p> <p>Department of Chemistry and Center of Novel Functional MoleculesThe Chinese University of Hong KongShatin New Territories Hong Kong SAR People's Republic of China;</p> <p>Department of Chemistry and Center of Novel Functional MoleculesThe Chinese University of Hong KongShatin New Territories Hong Kong SAR People's Republic of China;</p> <p>Department of Chemistry and Center of Novel Functional MoleculesThe Chinese University of Hong KongShatin New Territories Hong Kong SAR People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=cluster compounds&option=203" rel="nofollow">cluster compounds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal-organic frameworks&option=203" rel="nofollow">metal-organic frameworks;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=silver thiolate&option=203" rel="nofollow">silver thiolate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supramolecular chemistry&option=203" rel="nofollow">supramolecular chemistry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=X-ray crystallography&option=203" rel="nofollow">X-ray crystallography;</a> </p> <div class="translation"> 机译：簇化合物;金属有机框架;银硫醇盐;超分子化学;X射线晶体学; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022087076.html">Silver Thiolate Nano‐sized Molecular Clusters and Their Supramolecular Covalent Frameworks: An Approach Toward Pre‐templated Synthesis</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Zi‐Yi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Chen Zi‐Yi,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Tam Dennis Y. 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