Characterization of Porous Silica Materials with?Water at Ambient Conditions. Calculating the Pore Size Distribution from the Excess Surface Work Disjoining Pressure Model

Georgi Nikolaj; Kolesnikov Andrei; Uhlig Hans; M?llmer Jens; Rückriem Michael; Schreiber Andreas; Adolphs Jürgen; Enke Dirk; Gl?ser Roger

摘要

Abstract >Characterization of mesoporous materials today is routinely performed recording the adsorption isotherm of nitrogen at 77?K. The pore size distribution (PSD) can subsequently be determined using either thermodynamics or statistical mechanics based approaches. While nitrogen has evolved as the reference adsorptive, other gases are often used to extract more information from the isotherm. This contribution is focused on the calculation of a PSD from the water vapor isotherm. It is demonstrated that water adsorption provides accurate results comparable to the standard nitrogen adsorption. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >表征今天的中孔材料经常在77 k下记录氮的吸附等温线。随后可以使用基于热力学或基于统计力学的方法来确定孔径分布（PSD）。虽然氮气已经发展为参考吸附，但是其他气体通常用于从等温线中提取更多信息。该贡献专注于从水蒸气等温线计算PSD。结果表明，水吸附提供了与标准氮吸附相当的准确结果。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16114/'>《Chemie-Ingenieur-Technik: Verfahrenstechnik Technische Chemie Apparatewesen Biotechnologie》</a> <b style="margin: 0 2px;">|</b><span>2017年第12期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Georgi Nikolaj&option=202" target="_blank" rel="nofollow">Georgi Nikolaj;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kolesnikov Andrei&option=202" target="_blank" rel="nofollow">Kolesnikov Andrei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Uhlig Hans&option=202" target="_blank" rel="nofollow">Uhlig Hans;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=M?llmer Jens&option=202" target="_blank" rel="nofollow">M?llmer Jens;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rückriem Michael&option=202" target="_blank" rel="nofollow">Rückriem Michael;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Schreiber Andreas&option=202" target="_blank" rel="nofollow">Schreiber Andreas;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Adolphs Jürgen&option=202" target="_blank" rel="nofollow">Adolphs Jürgen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Enke Dirk&option=202" target="_blank" rel="nofollow">Enke Dirk;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gl?ser Roger&option=202" target="_blank" rel="nofollow">Gl?ser Roger;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>GMBU – Gesellschaft zur F?rderung von Medizin- Bio- und Umwelttechnologien e.V.Erich-Neu?-Weg 5 06120 Halle (Saale) Germany;</p> <p>Institut für Nichtklassische Chemie e.V.Permoserstra?e 15 04318 Leipzig Germany;</p> <p>Institut für Nichtklassische Chemie e.V.Permoserstra?e 15 04318 Leipzig Germany;</p> <p>Institut für Nichtklassische Chemie e.V.Permoserstra?e 15 04318 Leipzig Germany;</p> <p>POROTEC GmbH Niederhofheimer Stra?e 55A 65719 Hofheim am Taunus Germany;</p> <p>POROTEC GmbH Niederhofheimer Stra?e 55A 65719 Hofheim am Taunus Germany;</p> <p>POROTEC GmbH Niederhofheimer Stra?e 55A 65719 Hofheim am Taunus Germany;</p> <p>Fakult?t für Chemie und Mineralogie Institut für Technische ChemieUniversit?t LeipzigLinnèstra?e 3 04103 Leipzig Germany;</p> <p>Institut für Nichtklassische Chemie e.V.Permoserstra?e 15 04318 Leipzig Germany;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/238.html" title="化学工业">化学工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Density functional theory&option=203" rel="nofollow">Density functional theory;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Excess surface work&option=203" rel="nofollow">Excess surface work;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=MCM‐41&option=203" rel="nofollow">MCM‐41;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pore size distribution&option=203" rel="nofollow">Pore size distribution;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Water adsorption&option=203" rel="nofollow">Water adsorption;</a> </p> <div class="translation"> 机译：密度函数理论;过度的表面工作;MCM-41;孔径分布;水吸附; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div 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