Simultaneous Multiplex Potentiostatic Electroanalysis with Liquid‐Junction‐Removed Reference Electrode System using a Closed Bipolar Electrode

Inoue Kumi Y.; Ikegawa Miho; Ito‐Sasaki Takahiro; Takano Shinichiro; Shiku Hitoshi; Matsue Tomokazu

摘要

Abstract >A novel liquid‐junction‐removed reference electrode system was developed for simultaneous multiplex amperometry using a closed bipolar electrode. The liquid junction between the reference cell and the sample cell was replaced by a bipolar electrode to ensure electron conductivity in lieu of ionic conductivity in conventional systems. Under the condition where the redox reaction of the analyte at the bipolar electrode in the sample cell was a limiting process, voltammetric and amperometric measurements were performed for quantitative detection of the analytes. After characterization of the system, a chip‐type device was fabricated with six sample cells and one reference cell. Simultaneous determination of ferrocene methanol was conducted in six solutions in the 0.1–0.5?mM range. This is the first demonstration of the simultaneous multiplex determination of analytes with a liquid‐junction‐removed system. Although the potential control problem (which is different to the liquid potential problem of conventional liquid junction) still remains because of the increase of the solid–liquid interface, this system is expected to solve some problems associated with the liquid junction of the reference electrode, including sample contamination by chloride ions and the complicated process of fabricating a reference electrode on a chip. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <标题类型=“main”>抽象</ title> >使用闭合双极电极同时复用amperometry开发了一种新型液体结去除去的参考电极系统。通过双极电极代替参考电池和样品电池之间的液体结，以确保电子传导性代替常规系统中的离子电导率。在样品细胞中双极电极在双极电极的氧化还原反应是限制过程的条件下，进行伏安和慢性测量来进行分析物的定量检测。在系统表征之后，用六个样品细胞和一个参考单元制造芯片型器件。同时测定二茂铁甲醇的六个溶液在0.1-0.5Ωmm范围内进行。这是第一次演示通过液态结 - 去除系统同时复用的分析物的测定。尽管潜在的控制问题（与传统液体结的液体电位问题不同）仍然是由于固体液体界面的增加而仍然存在，但是该系统预计将解决与参比电极的液体结相关的一些问题，包括氯离子的样品污染和在芯片上制造参比电极的复杂过程。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16042/'>《ChemElectroChem》</a> <b style="margin: 0 2px;">|</b><span>2018年第16期</span><b style="margin: 0 2px;">|</b><span>共4页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Inoue Kumi Y.&option=202" target="_blank" rel="nofollow">Inoue Kumi Y.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ikegawa Miho&option=202" target="_blank" rel="nofollow">Ikegawa Miho;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ito‐Sasaki Takahiro&option=202" target="_blank" rel="nofollow">Ito‐Sasaki Takahiro;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Takano Shinichiro&option=202" target="_blank" rel="nofollow">Takano Shinichiro;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shiku Hitoshi&option=202" target="_blank" rel="nofollow">Shiku Hitoshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Matsue Tomokazu&option=202" target="_blank" rel="nofollow">Matsue Tomokazu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11 Aoba Aramaki Aoba Sendai 980-8579 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=closed bipolar electrode systems&option=203" rel="nofollow">closed bipolar electrode systems;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrode chips&option=203" rel="nofollow">electrode chips;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electroanalysis&option=203" rel="nofollow">electroanalysis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemical sensors&option=203" rel="nofollow">electrochemical sensors;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=liquid junctions&option=203" rel="nofollow">liquid junctions;</a> </p> <div class="translation"> 机译：闭合双极电极系统;电极碎片;电解分析;电化学传感器;液态线电片; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022061691.html">Simultaneous Multiplex Potentiostatic Electroanalysis with Liquid‐Junction‐Removed Reference Electrode System using a Closed Bipolar Electrode</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Inoue Kumi Y.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Inoue Kumi Y.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ikegawa Miho&option=202" target="_blank" rel="nofollow" class="tuijian_auth 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href="/journal-cn-9051/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 腐蚀与防护 </a> </span> <span> . 2011</span><span>,第011期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-35671_thesis/020221338050.html">使用Ｋｅｌｖｉｎ探头参比电极技术研究薄液层下氧还原反应</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王佳&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王佳</a> <span> <a href="/conference-cn-35671/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国腐蚀与防护学会建会十五周年学术年会 </a> <span> <span> . 1994</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313735922.html">阳极氧化法提高锌参比电极在海水中电位稳定性研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=孔祥超&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 孔祥超</a> <span> . 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