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首页> 外文期刊>ChemElectroChem >Anodic Oxidation of Ethynylferrocene Derivatives in Homogeneous Solution and Following Anodic Deposition onto Glassy Carbon Electrodes
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Anodic Oxidation of Ethynylferrocene Derivatives in Homogeneous Solution and Following Anodic Deposition onto Glassy Carbon Electrodes

机译：均相溶液中乙炔基茂丙烯衍生物的阳极氧化，阳极沉积在玻碳电极上

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Abstract > Eight ferrocene derivatives linked by either an ether, amine, or phenylacetylene moiety to a terminal ethynyl group were covalently deposited on glassy carbon electrodes by anodic electrochemical methods. The lithio activation method, in which the terminal hydrogen of the ethynyl group is replaced by a lithium atom before anodic oxidation, was successfully employed in all cases. Direct oxidation of the inactivated ethynyl group also resulted in surface deposition. Surface coverages between 1×10 ?10 ?mol?cm ?2 and 14×10 ?10 ?mol?cm ?2 were achieved. Cyclic voltammetry scans of the modified electrodes in pure electrolytes differed depending on the size of the supporting electrolyte anion, as little as half the current being measured for a [B(C <sub>6</sub> F <sub>5</sub> ) <sub>4</sub> ] ? vs. [PF <sub>6</sub> ] ? solution, suggesting differences in ion transport near the electrode surface. An ether‐linked ethynylferrocenium ion ( 5 + ) was isolated after electrolytic and chemical oxidation of 5 and characterized by X‐Ray crystallography as its [SbCl <sub>6</sub> ] ? salt. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 通过阳极电化学方法将通过乙醚，胺或苯乙炔部分连接到末端乙炔基的八个二氧化烯衍生物通过阳极电化学方法在玻璃碳电极上共价沉积。在阳极氧化前通过锂原子代替乙炔基的末端氢的LithiO活化方法，在所有情况下成功使用。将灭活的乙炔基的直接氧化也导致表面沉积。表面覆盖范围在1×10之间 ？10 </ sup> ？摩尔？cm ？2 </ sup> 和14×10 ？10 </ sup> ？摩尔？cm ？2 </ sup> 实现了。纯电解质中修饰电极的循环伏安法扫描根据支撑电解质阴离子的尺寸而不同，只要测量的电流的一半（C） <sub> 6 </ sub> F <sub> 5 </ sub> 的） <sub> 4 </ sub> ] ？</ sup> vs. [PF. <sub> 6 </ sub> ] ？</ sup> 解决方案，建议电极表面附近离子输送的差异。醚连接的乙炔比二烯酮离子（ 5 </ b> + </ sup> 电解和化学氧化后被隔离 5 </ b> 并以X射线晶体学为特征作为其[SBCL <sub> 6 </ sub> ] ？</ sup> 盐。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16042/'>《ChemElectroChem》</a> <b style="margin: 0 2px;">|</b><span>2019年第23期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sheridan Matthew V.&option=202" target="_blank" rel="nofollow">Sheridan Matthew V.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lam Kevin&option=202" target="_blank" rel="nofollow">Lam Kevin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Waterman Rory&option=202" target="_blank" rel="nofollow">Waterman Rory;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Geiger William E.&option=202" target="_blank" rel="nofollow">Geiger William E.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryUniversity of VermontBurlington Vermont 05495 U.S.A.;</p> <p>Department of ChemistryUniversity of VermontBurlington Vermont 05495 U.S.A.;</p> <p>Department of ChemistryUniversity of VermontBurlington Vermont 05495 U.S.A.;</p> <p>Department of ChemistryUniversity of VermontBurlington Vermont 05495 U.S.A.;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemical deposition&option=203" rel="nofollow">electrochemical deposition;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ferrocene&option=203" rel="nofollow">ferrocene;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ethynyl group&option=203" rel="nofollow">ethynyl group;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrolytes&option=203" rel="nofollow">electrolytes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=large anions&option=203" rel="nofollow">large anions;</a> </p> <div class="translation"> 机译：电化学沉积;二茂铁;乙炔基;电解质;大阴离子; 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J. </a> <span>1979</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：玻碳电极在差分脉冲阳极溶出伏安法（DpasV）中测定河水中汞的应用</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_plating-finishing_thesis/0201245478254.html">铝在硫酸溶液中的复合阳极氧化研究Ⅳ. 添加SiC粉体硫酸溶液中铝的阳极氧化工艺</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=罗胜联&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 罗胜联</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曾祥勇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曾祥勇</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=旷亚非&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,旷亚非</a> <span> <a href="/journal-cn-9045/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 电镀与精饰 </a> </span> <span> . 2002</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201297594351.html">铝的多孔型膜在(NH_4)_2MoS_4水溶液中二次阳极氧化时膜的生长机理 Ⅰ.二次阳极氧化过程中孔中溶液酸度变化对V—t曲线的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘海平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘海平</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=徐源&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,徐源</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张文奇&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,张文奇</a> <span> <a href="/journal-cn-57155/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国腐蚀与防护学报 </a> </span> <span> . 1990</span><span>,第2期</span> </span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/academic-journal-cn_china-foreign-medical-treatment_thesis/0201248402214.html">氢化偶联反应--用硼氢化钠阳极氧化法使乙炔衍生物电化学偶联</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王瑞芝&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 王瑞芝</a> <span> <a href="/journal-cn-6606/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中外医疗 </a> </span> <span> . 2001</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-journal-cn_plating-finishing_thesis/0201245479487.html">铝在硫酸溶液中的复合阳极氧化研究Ⅱ. 难溶粉体的细度对阳极氧化的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=许岩&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 许岩</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=旷亚非&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,旷亚非</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曾凌三&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曾凌三</a> <span> <a href="/journal-cn-9045/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 电镀与精饰 </a> </span> <span> . 2001</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_plating-finishing_thesis/0201245480936.html">铝在硫酸溶液中的复合阳极氧化研究Ⅲ难溶粉体预处理对阳极氧化的影响</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=周海晖&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 周海晖</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=旷亚非&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,旷亚非</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曾凌三&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曾凌三</a> <span> <a href="/journal-cn-9045/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 电镀与精饰 </a> </span> <span> . 2001</span><span>,第006期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-1024_thesis/0202247122.html">聚丙烯腈(PAN)基碳纤维的表面阳极氧化原理研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=QIAN Xin&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . QIAN Xin</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=钱鑫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,钱鑫</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZHANG Yong-gang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,ZHANG Yong-gang</a> <span> <a href="/conference-cn-1024/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国工程科技论坛暨2015年（萧山）中国纺织工程学会化纤专业委员会学术年会 </a> <span> <span> . 2015</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/02031764656.html">苯乙炔基吡啶衍生物在酸性水溶液中的光环加成反应研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=程鑫&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 程鑫</a> <span> . 2009</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120103241332.html">用于阳极氧化层中降低的染料吸收的染料溶液替代物</a> <b>[P]</b> . <span> 中国专利： CN110835774A </span> <span> . 2020-02-25</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120100290992.html">一种硫酸-草酸混合酸硬质阳极氧化溶液中硫酸含量的测定方法</a> <b>[P]</b> . <span> 中国专利： CN109212124A </span> <span> . 2019-01-15</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130439398451.html">METHOD FOR FORMING OXIDE ANODE OF ORGANIC ELECTROLUMINESCENCE DEVICE, INCLUDING STEPS OF FORMING DOPED OXIDE ELECTRODE LAYER ON SUBSTRATE AND FORMING SURFACE OXIDE LAYER ON OXIDE ELECTRODE LAYER THROUGH ATOMIC LAYER DEPOSITION PROCESS, AND ORGANIC ELECTROLUMINESCENCE DEVICE INCLUDING OXIDE ANODE LAYER</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20040103672A </span> <span> . 2004-12-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：形成有机电致发光装置的氧化物阳极的方法，包括在基质上形成掺杂的氧化物电极层并通过氧化物层沉积方法在氧化物电极层上形成氧化物表面的有机氧化物层的步骤，以及有机合成方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130453458694.html">Liquid crystal display device with tfts in which pixel electrodes are formed in the same plane as the gate electrodes with anodized oxide films before the deposition of silicon</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US5402254B1 </span> <span> . 1998-09-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：具有tft的液晶显示装置，其中在沉积硅之前，在与具有阳极氧化膜的栅电极相同的平面中形成像素电极 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130455004616.html">LCD device with TFTs in which pixel electrodes are formed in the same plane as the gate electrodes with anodized oxide films and before the deposition of the silicon gate insulator</a> <b>[P]</b> . <span> 外国专利： <!-- 美国专利： --> US5671027A </span> <span> . 1997-09-23</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：带有TFT的LCD器件，其中像素电极与带有阳极氧化膜的栅电极形成在同一平面中，并且在沉积硅栅绝缘体之前 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704022060694','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img 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