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Synthesis and characterization of Znq2 and Znq2:CTAB particles for optical applications

机译:ZnQ2和ZnQ2的合成与表征:光学应用的CTAB粒子

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High luminescent zinc (ii)-bis (8-hydroxyquinoline) Znq2 nanoparticles were synthesized by the simple precipitation method in pure form and with cetyltrimethyl ammonium bromide (CTAB) as cationic surfactant. The crystalline nature of title samples was confirmed by powder X-ray diffraction. Thermo gravimetric analysis and differential thermal analysis were carried out to find the thermal stability of the synthesized samples. The morphology and elemental analyses of the samples were studied by scanning electron microscope and energy dispersive X-ray analyser, respectively. The functional groups of these nanoparticles were analysed and assigned using the Fourier transform infrared spectroscopy spectral study. The optical property of Znq2 and Znq2:CTAB was confirmed by UV-vis-NIR spectral study. The band gap of Znq2 was calculated. The synthesized Znq2 and Znq2:CTAB nanoparticles were confirmed by photoluminescence studies for organic-light-emitting diode applications as emission and electron transport layers.
机译:通过纯形式的简单沉淀法和用甲基三亚甲基溴化物(CTAB)作为阳离子表面活性剂,通过简单的沉淀法合成高发亮锌(II)ZnQ2纳米颗粒。通过粉末X射线衍射证实标题样品的结晶性质。进行热重量分析和差分热分析以找到合成样品的热稳定性。通过扫描电子显微镜和能量分散X射线分析仪研究样品的形态和元素分析。使用傅里叶变换红外光谱分谱研究分析和分配这些纳米颗粒的官能团。通过UV-Vis-niR光谱研究证实了ZnQ2和ZnQ2的光学性能:CTAB。计算ZnQ2的带隙。合成的ZnQ2和ZnQ2:CTAB纳米颗粒通过光致发光研究证实了用于有机发光二极管应用作为发射和电子传输层。

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