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Environmental friendly approach for facile synthesis of graphene-like nanosheets for photocatalytic activity

机译:用于光催化活性的石墨烯纳米片的环境友好方法

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Here, an environmentally friendly bottom-up method introduced as an easy, inexpensive, and affordable method for synthesize of graphene-like nanostructures. Results indicated that the presence of FeCl3 and oxalic acid could improve the quality of the final product impressively. FeCl3 plays key role for the generation of the high-quality graphene because it acts as both template and catalyst for the formation of graphene. The products were characterized by XRD, FT-IR, TGA, SEM, Raman and TEM analyses. The photocatalytic degradation ability of (graphene/iron oxide/titanium dioxide) Gr/Fe3O4/TiO2 nanocomposite for the removal of rhodamine B dyes from wastewater was reported. The obtained adsorbent with porous structure not only exhibited fast adsorption rate, superior adsorption capacity, but also presented convenient magnetic separation characteristic. Synthesized magnetic nanostructures can be separated from reaction mixtures by an external magnet. As a result of its attractive features such as; simple preparation, superior catalytic activity and magnetic recyclability the synthesized nanocomposite obtained in this work provides a new insight to enhance the photocatalytic efficiency. (C) 2020 Elsevier B.V. All rights reserved.
机译:这里,环保自下而上的方法作为合成石墨烯纳米结构的简单,廉价,价格实惠的方法。结果表明,FECL3和草酸的存在可能令人印象深刻地提高最终产品的质量。 FECL3为生成高质量石墨烯发挥关键作用,因为它充当用于形成石墨烯的模板和催化剂。该产品的特点是XRD,FT-IR,TGA,SEM,拉曼和TEM分析。报道了(石墨烯/氧化铁/二氧化钛)GR / Fe3O4 / TiO2纳米复合材料用于除去废水中罗丹明B染料的光催化降解能力。具有多孔结构的获得的吸附剂不仅表现出快速吸附速率,优异的吸附能力,而且还呈现了方便的磁分离特性。合成的磁性纳米结构可以通过外部磁铁与反应混合物分离。由于其具有吸引力的特征,如;简单的制备,优异的催化活性和磁性再循环性本工作中获得的合成纳米复合材料提供了新的洞察力,以提高光催化效率。 (c)2020 Elsevier B.v.保留所有权利。

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