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Investigation of Vacuum Hot-Press Sintering Temperatures on the Sintered Characteristics of Cr-31.2 mass% Ti Alloys

机译:CR-31.2质量%Ti合金烧结特性真空热压烧结温度的研究

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The aim of this work is to find the optimal sintering parameters of Cr-31.2 mass% Ti alloys and simultaneously investigate the effects of the TiCr2 Laves phases. In this study, Cr-31.2 mass% Ti alloys are fabricated by vacuum hot-press sintering. Different compositions of submicron titanium (760 nm) powders are added to micron chromium (4.66 mu m) powders. The experiments utilize various hot-press sintering temperatures (1250, 1300, 1350 and 1400 degrees C) with the pressure maintained at 20 MPa for 1 h, respectively. The experimental results show the optimal parameters of the hot-press sintered Cr-31.2 mass% Ti alloys to be 1400 degrees C at 20 MPa for 1 h. The relative density reaches 99.96% and the hardness and TRS (transverse rupture strength) reach 81.93 HRA and 475.73 MPa, respectively. In addition, the increase in temperature of the hot-press sintering is effectively decreased the Cr3Ti3O and slightly enhanced TiCr2 phases, which will lead to the better mechanical properties. Significantly, the optimal hot-press sintered Cr-31.2 mass% Ti alloys possess a dense microstructure, excellent mechanical property and good electrical conductivity value (1.51 x 10(4) S cm(-1)).
机译:这项工作的目的是找到Cr-31.2质量%Ti合金的最佳烧结参数,并同时研究TiCr2 Laves阶段的影响。在本研究中,CR-31.2质量%Ti合金通过真空热压烧结制造。将亚微米钛(760nm)粉末的不同组成加入微米铬(4.66μm)粉末中。该实验利用各种热压烧结温度(1250,1300,1350和1400℃),压力分别保持在20MPa的1小时。实验结果表明,热压烧结CR-31.2质量%Ti合金的最佳参数为1400℃,为20MPa 1小时。相对密度达到99.96%,硬度和TRS(横向断裂强度)分别达到81.93HRA和475.73MPa。此外,热压烧结的温度的增加有效地降低了Cr3Ti3O和略微增强的TiCr2阶段,这将导致更好的机械性能。值得注意的是,最佳的热压烧结Cr-31.2质量%Ti合金具有致密的微观结构,优异的机械性能和良好的电导率值(1.51×10(4)厘米(-1))。

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