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首页> 外文期刊>Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics >Processing and microstructure characterization of SiCp/Hastelloy(Ni-Mo-Cr) composites prepared by pressureless infiltration
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Processing and microstructure characterization of SiCp/Hastelloy(Ni-Mo-Cr) composites prepared by pressureless infiltration

机译:无压浸渗法制备SiCp / Hastelloy(Ni-Mo-Cr)复合材料的工艺及组织表征

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摘要

SiCp/Hastelloy composites were fabricated by pressureless Ti-activated infiltration process. The wetting and infiltration behaviors of Hastelloy on the SiC substrates and the interfacial reaction between the SiC particles and Hastelloy were investigated by real-time observation system, X-ray diffraction (XRD) and scanning electron microscopy (SEM) equipped with energy X-ray dispersive spectroscopy (EDS) system. The results demonstrated that the Hastelloy had a good wettability on SiC ceramic and could spontaneously infiltrate into the Ti-activated SiC preform. Moreover, intensive interfacial reaction similar to SiC/Ni system was found between the SiC particles and Hastelloy, which induced defects in the microstructure. In order to inhibit the interfacial reaction, Al2O3 coating on SiC particles was adopted as a diffusion barrier, which effectively reduced the extent of the interfacial reactions. (C) 2015 Elsevier B. V. All rights reserved.
机译:SiCp / Hastelloy复合材料是通过无压Ti活化渗透工艺制备的。通过实时观察系统,X射线衍射(XRD)和配备能量X射线的扫描电子显微镜(SEM)研究了哈氏合金在SiC衬底上的润湿和渗透行为以及SiC颗粒与哈氏合金之间的界面反应。色散光谱(EDS)系统。结果表明,哈氏合金在SiC陶瓷上具有良好的润湿性,并且可以自发渗入Ti活化的SiC预成型坯中。此外,在SiC颗粒和Hastelloy之间发现了类似于SiC / Ni体系的强烈界面反应,这引起了微观结构的缺陷。为了抑制界面反应,采用SiC颗粒上的Al2O3涂层作为扩散阻挡层,有效降低了界面反应的程度。 (C)2015 Elsevier B. V.保留所有权利。

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