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Preparation and properties of atomic oxygen protective films deposited on Kapton by solvothermal and sol-gel methods

机译:溶剂热和溶胶-凝胶法在Kapton上沉积原子氧保护膜的制备及性能

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摘要

Due to a smooth hydrophobic surface of Kapton, it is very difficult for other materials to bond to it. In this study, using solvothermal method to modify the surface of Kapton substrates, the adhesion between silica film and Kapton substrate was greatly improved. Silica films were prepared on Kapton substrate via sol-gel method and the samples were irradiated by atomic oxygen (AO) in a ground-based simulation system. The AO erosion yield values of the samples after AO irradiation were tested. The surface morphology and the structure of silica films were investigated by scanning electronic microscope (SEM) and Fourier transformed infrared spectroscopy (FTIR). The results indicated that a uniform thin film was easily formed on the surface of Kapton. After AO exposure, the silica films become smoother and more uniform, without peeling off, and the AO erosion yield of coated Kapton was sharply down, equivalent to only 4.7% of pristine Kapton.
机译:由于Kapton的疏水表面光滑,其他材料很难与之粘合。本研究采用溶剂热法对Kapton基材表面进行改性,大大提高了二氧化硅膜与Kapton基材之间的附着力。通过溶胶-凝胶法在Kapton基板上制备二氧化硅薄膜,并在基于地面的模拟系统中用原子氧(AO)照射样品。测试了样品在AO辐照后的AO腐蚀屈服值。通过扫描电子显微镜(SEM)和傅里叶变换红外光谱(FTIR)研究了二氧化硅膜的表面形态和结构。结果表明在Kapton的表面上容易形成均匀的薄膜。暴露于AO后,二氧化硅膜变得更光滑,更均匀,没有剥落,涂层的Kapton的AO侵蚀率急剧下降,仅相当于原始Kapton的4.7%。

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