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Effect of annealing on the microstructure and erosion performance of cold-sprayed FeAl intermetallic coatings

机译:退火对冷喷涂FeAl金属间化合物涂层组织和腐蚀性能的影响

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摘要

FeAl intermetallic coatings were prepared by cold spraying of mechanically alloyed metastable Fe(Al) powder assisted with post-spray annealing treatment. The microstructure evolution and erosion performance of the coatings annealed at different temperatures were investigated and the erosion mechanism of the intermetallic coatings was examined through the surface morphology and cross-sectional microstructure of the eroded coatings. After annealing at 650°C, the heterogeneous feature in the as-sprayed coating was evidently modified. With annealing temperature rising to 950°C and 1100°C, the interfaces between the particles in the coating completely disappeared. The erosion rate of the coating at the erosion angles of both 30o and 90o decreased with the increase in the annealing temperature. It was found that the erosion resistance of the intermetallic coating annealed at 1100°C was three times higher than that of the as-sprayed coating. The weight loss of the as-sprayed coating with low cohesion at erosion angle of 90° was attributed to particle spalling off. The weight loss of the annealed intermetallic coatings with enhanced cohesion was attributed to microcutting and ploughing of erosive particles.
机译:FeAl金属间化合物涂层是通过对机械合金化的亚稳态Fe(Al)粉末进行冷喷涂,并辅以后喷涂退火处理而制备的。研究了在不同温度下退火的涂层的组织演变和腐蚀性能,并通过腐蚀后的涂层的表面形貌和横截面微观结构,研究了金属间化合物的腐蚀机理。在650°C退火后,喷涂后的涂层中的异质特征得到明显修饰。随着退火温度升高到950℃和1100℃,涂层中的颗粒之间的界面完全消失。随着退火温度的升高,在30o和90o腐蚀角下的涂层腐蚀速率均降低。发现在1100℃下退火的金属间化合物涂层的耐蚀性比喷涂后的涂层高三倍。在90°侵蚀角下具有低内聚力的喷涂涂层的重量损失归因于颗粒剥落。具有增强的内聚力的退火金属间化合物涂层的重量损失归因于侵蚀颗粒的微切割和耕作。

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