C-H Hydroxylation of Phosphonates with Oxygen in [bmIm]OH To Produce Quaternary alpha-Hydroxy Phosphonates

Li Xiangguang; Jin Cheng; Gu Lijun

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C-H Hydroxylation of Phosphonates with Oxygen in [bmIm]OH To Produce Quaternary alpha-Hydroxy Phosphonates

机译：在[bmIm] OH中用氧气对膦酸酯进行C-H羟基化反应以生成季α-羟基膦酸酯

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A highly efficient and mild [bmIm]OH-catalyzed a-hydroxylation of phosphonates using O-2 as the oxygen source is described. The employment of ionic liquid under mild reaction conditions makes this transformation green and practical. Especially, this reaction provided a novel and convenient methodology for the construction of quaternary a-hydroxy phosphonates.

机译：描述了使用O-2作为氧源的高效且温和的[bmIm] OH催化的膦酸酯的α-羟基化。在温和的反应条件下使用离子液体使这种转化绿色而实用。特别地，该反应为构建季α-羟基膦酸酯提供了新颖且方便的方法。

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《The Journal of Organic Chemistry》 |2015年第4期|共5页
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Li Xiangguang; Jin Cheng; Gu Lijun;
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1. C-H Hydroxylation of Phosphonates with Oxygen in [bmIm]OH To Produce Quaternary alpha-Hydroxy Phosphonates [J] . Li Xiangguang, Jin Cheng, Gu Lijun The Journal of Organic Chemistry . 2015,第4期

机译：在[bmIm] OH中用氧气对膦酸酯进行C-H羟基化反应以生成季α-羟基膦酸酯
2. The catalytic aerobic synthesis of quaternary alpha-hydroxy phosphonates via direct hydroxylation of phosphonate compounds [J] . Gu Lijun, Jin Cheng, Zhang Hongtao New Journal of Chemistry . 2015,第3期

机译：通过膦酸酯化合物的直接羟基化催化有氧合成季α-羟基膦酸酯
3. Synthesis of Quaternary α-Hydroxy Phosphonates via Direct Hydroxylation of Phosphonate Compounds [J] . Jiyan Liu, Wei Wang, Rui Wang, 中国化学（英文版） . 2015,第005期

机译：通过膦酸酯化合物的直接羟基化反应合成α-羟基膦酸酯
4. The Relation Between Barite Inhibition by Phosphonate Scale Inhibitors and the Structures of Phosphonate-Metal Complexes [C] . S.S. Shaw, T.D. Welton, K.S. Sorbie Society of Plastics Engineers International Conference and Exhibition on Oilfield Scale . 2012

机译：膦酸盐尺度抑制剂与膦酸盐 - 金属配合物结构之间的关系
5. The stereoselective synthesis of alpha-hydroxy phosphonates: Applications in the synthesis of heterocyclic compounds. [D] . He, Anyu. 2005

机译：α-羟基膦酸酯的立体选择性合成：在杂环化合物合成中的应用。
6. Coordination Behavior of 14-Disubstituted Cyclen Endowed with Phosphonate Phosphonate Monoethylester and H-Phosphinate Pendant Arms [O] . Jiří Bárta, Petr Hermann, Jan Kotek 2019

机译：带有膦酸酯膦酸酯单乙酯和H-膦酸酯悬挂臂的14-二取代环素的配位行为
7. Copper-Catalyzed Synthesis of alpha-Hydroxy Phosphonates from H-Phosphonates and Alcohols or Ethers [O] . Zhao Zengxiang, Xue Wanhua, Gao Yuxing, 2013

机译：铜催化的H-膦酸酯和醇或醚合成α-羟基膦酸酯
8. Amino Phosphonate and Amino Bis-Phosphonate Derivatives. [R] . Petasis, N. A. 2004

机译：氨基膦酸酯和氨基双膦酸酯衍生物。

C-H Hydroxylation of Phosphonates with Oxygen in [bmIm]OH To Produce Quaternary alpha-Hydroxy Phosphonates

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