Facile one-pot synthesis of 2,3-thienoimides via formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides

Shi Wenjuan; Sun Shaofa; Hu Yimin; Gao Tao; Peng Yanhong; Wu Minghu; Guo Haibing; Wang Jian

首页> 外文期刊>Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry >Facile one-pot synthesis of 2,3-thienoimides via formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides

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Facile one-pot synthesis of 2,3-thienoimides via formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides

机译：通过1,4-二噻吩-2,5-二醇与N-取代的酰亚胺的正式[3 + 2]环化反应，轻松地一锅合成2,3-硫代酰亚胺

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摘要

A formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides through one-pot metal-free strategy has been developed. This method could furnish 2,3-thienoimides in good to high yields. (C) 2015 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2015年第25期|共3页
作者
Shi Wenjuan; Sun Shaofa; Hu Yimin; Gao Tao; Peng Yanhong; Wu Minghu; Guo Haibing; Wang Jian;
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正文语种 eng
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关键词
3+2-Cycloaddition; 1; 4-Dithiane-2; 5-diol; Imide; Thiophene;

机译：[3 + 2]-环加成;1;4-二噻二-2;5-二醇;亚胺;噻吩;

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1. Facile one-pot synthesis of 2,3-thienoimides via formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides [J] . Shi Wenjuan, Sun Shaofa, Hu Yimin, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第25期

机译：通过1,4-二噻吩-2,5-二醇与N-取代的酰亚胺的正式[3 + 2]环化反应，轻松地一锅合成2,3-硫代酰亚胺
2. Facile synthesis of 3-aldehyde-2-substituted thiophenes through Lewis base catalyzed [3+2] cycloaddition of 1,4-dithiane-2,5-diols with ynals [J] . Shi Wenjuan, Wan Li, Hu Yimin, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第16期

机译：通过Lewis碱催化的1，4-二硫代-2,5-二醇与烯醛的[3 + 2]环加成反应，可轻松合成3-醛-2-取代的噻吩
3. Organocatalytic asymmetric [3+2] annulation of 1,4-dithiane-2,5-diol with azlactones: access to chiral dihydrothiophen-2(3H)-one derivatives [J] . Yu Ji-cong, Yu Le-mao, Zhao Xiao-yun, Organic Chemistry Frontiers . 2018,第13期

机译：有机催化的不对称[3 + 2]用唑类药物的1,4-二碘-2,5-二醇的环节：进入手性二氢噻吩-2（3h） - 酮衍生物
4. Facile Synthesis of Dendralenes Based on the Cross-coupling Reaction of 1,1-Diborylethene and 2,3-Diboryl-l,3-butadiene [C] . Masaki Shimizu, Kei Tanaka, Takuya Kurahashi, Symposium on Organometallic Chemistry . 2003

机译：基于1,1-二苯甲酸乙烯的交叉偶联反应和2,3-二硼乙烯-1，3-丁二烯的树枝状的体内合成
5. (3+2) Annulation Reactions of Azaoxyallyl Cations: Synthesis of Pyrroloindolines and Imidazolones [D] . DiPoto, Maria C. 2018

机译：（3 + 2）氮氧基烯丙基阳离子的环化反应：吡咯啉二环和咪唑酮的合成
6. Synthesis of (+)-Bullatacin via the Highly Diastereoselective 3+2 Annulation Reaction of a Racemic Aldehyde and a Non-Racemic Allylsilane [O] . Jennifer M. Tinsley, Eric Mertz, Pek Y. Chong, -1

机译：外消旋醛与非外消旋烯丙基硅烷的高度非对映选择性3 + 2环合反应合成（+）-布拉他星
7. Correction: A metal-free cascade reaction of β-halo-α,β-unsaturated aldehydes and 1,4-dithiane-2,5-diols: synthesis of polycyclic 2-formylthiophenes [O] . Limi Goswami, Kashmiri Neog, Kumud Sharma, 2019

机译：校正：β-卤素-α，β-不饱和醛和1,4-二硫醚-2,5-二醇的无金属级联反应：合成多环2-二甲苯烯酮

Facile one-pot synthesis of 2,3-thienoimides via formal [3+2] annulation reaction of 1,4-dithiane-2,5-diol and N-substituted imides

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