Nitrosation of beta'-hydroxylamino-alpha,beta-unsaturated oximes:synthesis of l,7-dioxa-2,6-diaza-spiro[4,4]nona-2,8-diene ring system

Ananda S.Amarasekara

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Nitrosation of beta'-hydroxylamino-alpha,beta-unsaturated oximes:synthesis of l,7-dioxa-2,6-diaza-spiro[4,4]nona-2,8-diene ring system

机译：β'-羟氨基-α，β-不饱和肟的亚硝化：1,7-二氧杂-2,6-二氮杂螺[4,4] nona-2,8-二烯环系统的合成

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Nitrosation of bis arylidene acetone oximes with nitrous acid in glacial acetic acid gives 3-vinyl pyrazolone-N,N'-dioxides in 32-37% yield.Similar reactions of 2-arylidene-6-(hydroxylamino-aryl-methyl)-cyclohexanone oximes give tricyclic compounds with dioxa-2,6-diaza-spiro[4,4] nona-2,8-diene ring systems in 77-84% yield.

机译：在冰醋酸中用亚硝酸亚硝基双亚芳基丙酮肟制得3-乙烯基吡唑啉酮-N，N'-二氧化物，收率为32-37％.2-亚芳基-6-（羟基氨基-芳基-甲基）-环己酮的类似反应肟以77-84％的收率得到具有dioxa-2,6-diaza-spiro [4,4] nona-2,8-diene环系统的三环化合物。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 》 |2005年第15期| 共4页
作者
Ananda S.Amarasekara;
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Nitrosation; alpha; beta-Unsaturated oximes; Pyrazolone; Dihydroisoxazole.;

机译：亚硝化;α;β-不饱和肟;吡唑啉酮;二氢异恶唑;

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1. Nitrosation of beta'-hydroxylamino-alpha,beta-unsaturated oximes:synthesis of l,7-dioxa-2,6-diaza-spiro[4,4]nona-2,8-diene ring system [J] . Ananda S.Amarasekara Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2005 ,第15期

机译：β'-羟氨基-α，β-不饱和肟的亚硝化：1,7-二氧杂-2,6-二氮杂螺[4,4] nona-2,8-二烯环系统的合成
2. Synthesis of Novel alpha,beta-Unsaturated Sulfonic Acid Derivatives Containing Dithiocarbamate/Xanthate Groups by Ring Opening of an alpha,beta-Unsaturated gamma-Sultone [J] . Foumeshi Maryam Khalili, Halimehjani Azim Ziyaei, Beier Petr Synlett . 2020 ,第10期

机译：通过α，β-不饱和γ-苏酮的环开口合成含有二硫代氨基甲磺酸酯/黄原酸酯基团的新型α，β-不饱和磺酸衍生物
3. Ring closure reactions of beta-nitroso-, beta-acyl-, and beta-thiocarbamoyl-alpha,beta-unsaturated sulfilimines. Synthesis of [1,2,5]oxadiazolo[3,4-d]-, isoxazolo[3,4-d]-, and isothiazolo[3,4-d]pyrimidine derivatives from uracils [J] . Matsumoto N., Takahashi M. Tetrahedron . 2002 ,第50期

机译：β-亚硝基-，β-酰基和β-硫代氨基甲酰基-α，β-不饱和亚硫酰亚胺的闭环反应。由尿嘧啶合成[1,2,5]恶二唑并[3,4-d]-，异恶唑并[3,4-d]-和异噻唑并[3,4-d]嘧啶衍生物
4. A New Approach to the Synthesis of 1,2,3-Triols Using alpha,beta-Unsaturated Acylsilanes [C] . Mitsunori Honda, Takayoshi Nakamura, Takumi Sumigawa Symposium on Organometallic Chemistry . 2007

机译：使用α，β不饱和酰基硅烷合成1,2,3-三醇的新方法
5. Part I. Reactions of alpha,beta-unsaturated thioesters and selenoesters with enamines. Part II. Alpha,beta-unsaturated thioesters and selenoesters as dienophiles: Synthesis of cyclohexene derivatives. [D] . Byeon, Chang-Ho. 1994

机译：第一部分：α，β-不饱和硫酯和硒酸酯与烯胺的反应。第二部分作为亲二烯体的α，β-不饱和硫代酸酯和硒酸酯：环己烯衍生物的合成。
6. Synthesis of 2H-furo23-cpyrazole ring systems through silver(I) ion-mediated ring-closure reaction [O] . Vaida Milišiūnaitė, Rūta Paulavičiūtė, Eglė Arbačiauskienė, 2019

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7. Diastereoselective cyclopropanation of medium and large ring alpha, beta-unsaturated homochiral ketals and enantioselective synthesis of (-)-modhephene. [O] . Math Shivanand Kumarswamy. 1989

机译：中大环α，β-不饱和同手性缩酮的非对映选择性环丙烷化和（-）-对苯二酚的对映选择性合成。
8. Synthesis and Dimerization 2,3-Dimethyl-5-Silaspiro(4,4)nona-2,7-diene [R] . Park, Y. T., Zhou, S. Q., Zhao, D., 1990

机译：合成和二聚化2,3-二甲基-5-硅杂螺（4,4）壬-2,7-二烯

Nitrosation of beta'-hydroxylamino-alpha,beta-unsaturated oximes:synthesis of l,7-dioxa-2,6-diaza-spiro[4,4]nona-2,8-diene ring system

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