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Preparation and characterization of silica-coated TiO2 nanoparticle

机译:二氧化硅包覆的TiO2纳米粒子的制备与表征

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In recent years. TiO2 nanoparticle complex has been increasingly utilized in sun care products because of its UV-ray shielding performance and chemical stability. TiO2 nanoparticles from Degussa (P-25) were used as a seed for SiO2 coating using TEOS. A SiO2-coated TiO2 nanoparticle was prepared by a sol-gel process. The high-resolution transmission electron microscope (HR-TEM), FT-IR, energy dispersion Spectrum (EDS) and X-ray photoelectron spectroscopy (XPS) analyses showed that the surface of TiO2 particles was evenly coated by amorphous SiO2 layer with 10-15 nm thickness. Coated particles were measured with X-ray powder diffraction (XRD) to know the heat treatment effect on crystal structure of SiO2 layer and TiO2 seed. (c) 2004 Elsevier B.V. All rights reserved.
机译:最近几年。 TiO2纳米粒子复合物因其紫外线屏蔽性能和化学稳定性而越来越多地用于防晒产品。来自德固赛公司(P-25)的TiO2纳米颗粒用作使用TEOS进行SiO2涂层的种子。通过溶胶-凝胶法制备了SiO 2包覆的TiO 2纳米颗粒。高分辨率透射电子显微镜(HR-TEM),傅立叶变换红外(FT-IR),能谱(EDS)和X射线光电子能谱(XPS)分析表明,TiO2颗粒的表面均匀地被10- 15 nm厚度。用X射线粉末衍射(XRD)测量被覆颗粒,以了解热处理对SiO2层和TiO2晶种晶体结构的影响。 (c)2004 Elsevier B.V.保留所有权利。

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