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Synthesis of titania-coated silica nanoparticles using a nonionic water-in-oil microemulsion

机译:非离子油包水型微乳液合成二氧化钛包覆的二氧化硅纳米粒子

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Titania-coated silica nanoparticles were prepared by controlled hydrolysis of tetraethoxysilane (TEOS) and titanium n-butoxide (TBOT) in Triton X-45/cyclohesane H2O reverse (water-in-oil) microemulsions. The pH of the microemulsion plays a key role in the coating of titania (TiO2) on silica (SiO2) nanoparticles. TiO2 loading up to 10 wt.% on SiO2 nanoparticles was detected by SEM-EDS. Quasielastic light scattering and transmission electron microscopy were used to characterize the size and morphology of synthesized nanoparticles. (C) 2001 Elsevier Science B.V. Ali rights reserved. [References: 29]
机译:通过在Triton X-45 /环己烷H2O反向(油包水)微乳液中四乙氧基硅烷(TEOS)和正丁醇钛(TBOT)的可控水解来制备二氧化钛包覆的二氧化硅纳米粒子。微乳液的pH在二氧化硅(SiO2)纳米颗粒上的二氧化钛(TiO2)涂层中起着关键作用。通过SEM-EDS检测到TiO 2在SiO 2纳米颗粒上的负载量高达10重量%。准弹性光散射和透射电子显微镜用于表征合成纳米粒子的大小和形态。 (C)2001 Elsevier Science B.V. Ali版权所有。 [参考:29]

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