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Reactive Commercial Ni/Al Nanolayers for Joining Lightweight Alloys

机译:用于连接轻质合金的反应性商用Ni / Al纳米层

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摘要

Reactive nanoscale multilayer foils for use in joining techniques have attracted a great deal of attention. A common feature of these nanolayers is the large amount of heat released during the reaction between the layers to form a new phase. In this study, films of alternated Ni and Al nanolayers (NanoFoil made by the Indium Corporation) with period (bilayer thickness) close to 54 nm and with a thickness of 60 μm were used as local heat sources to bond lightweight alloys. The as-deposited Ni and Al alternated nanolayers evolve into NiAl nanometric grains when the multilayer, ignited by an electrical discharge, reacts. Joining of lightweight alloys was performed at room temperature under pressures of 10-80 MPa. The ability of the nanolayers to join these alloys by high temperature diffusion bonding was also investigated. The micro-structural and chemical characterizations of the interfaces were performed on cross-sections of the joints by scanning electron microscopy and energy dispersive x-ray spectroscopy. Ni/Al nanolayers are an effective means of joining titanium alloys at room temperature. A sound interface, mainly composed by NiAl grains, is obtained in joints of TiAl/TiAl and TiAl/Inconel, produced with NanoFoil by annealing at 700℃, during 60 min under a pressure of 10 MPa. The low shear strength revealed a weak adhesion of the nanofoil to the base materials.
机译:用于连接技术的反应性纳米级多层箔引起了极大的关注。这些纳米层的共同特征是在各层之间的反应形成新相期间释放的大量热量。在本研究中,使用交替的Ni和Al纳米层(Indium Corporation制造的NanoFoil)的膜(周期厚度(双层厚度)接近54 nm,厚度为60μm)作为局部热源来粘结轻质合金。当由放电点燃的多层反应时,沉积的Ni和Al交替的纳米层演变成NiAl纳米晶粒。在室温下在10-80 MPa的压力下进行轻质合金的连接。还研究了纳米层通过高温扩散键合连接这些合金的能力。通过扫描电子显微镜和能量色散X射线光谱对接缝的横截面进行了界面的微观结构和化学表征。 Ni / Al纳米层是在室温下连接钛合金的有效方法。用NanoFoil在700℃退火,60分钟,10 MPa压力下产生的TiAl / TiAl和TiAl / Inconel的接头中获得了主要由NiAl晶粒组成的声音界面。低剪切强度显示出纳米箔与基础材料的弱粘合性。

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