High-Field and High-Speed CP-MAS ~(13)C NMR Heteronuclear Dipolar-Correlation Spectroscopy of Solids with Frequency-Switched Lee-Goldburg Homonuclear Decoupling

B. -J. van Rossum; H. Forster; H. J. M. de Groot

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High-Field and High-Speed CP-MAS ~(13)C NMR Heteronuclear Dipolar-Correlation Spectroscopy of Solids with Frequency-Switched Lee-Goldburg Homonuclear Decoupling

机译：高频率和高速CP-MAS〜（13）C NMR频率切换的Lee-Goldburg同核解耦固体异核双极相关光谱

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In this Communication, we demonstrate that the use of frequency-switched Lee-Goldberg irradiation during the proton evolution of fast-spinning 2-D heteronuclear ('H-13C correlation spectroscopy strongly enhances the proton resolution.

机译：在本通讯中，我们证明了在快速旋转的2-D异核（'H-13C相关光谱）的质子演化过程中使用频率切换的Lee-Goldberg辐照极大地提高了质子分辨率。

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《Journal of magnetic resonance》 |1997年第2期|共4页
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B. -J. van Rossum; H. Forster; H. J. M. de Groot;
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中图分类电磁学、电动力学;
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1. High-Field and High-Speed CP-MAS ~(13)C NMR Heteronuclear Dipolar-Correlation Spectroscopy of Solids with Frequency-Switched Lee-Goldburg Homonuclear Decoupling [J] . B. -J. van Rossum, H. Forster, H. J. M. de Groot Journal of magnetic resonance . 1997,第2期

机译：高频率和高速CP-MAS〜（13）C NMR频率切换的Lee-Goldburg同核解耦固体异核双极相关光谱
2. Simultaneous homonuclear and heteronuclear spin decoupling in magic-angle spinning solid-state NMR [J] . Mote Kaustubh R., Madhu Perunthiruthy K. Solid State Nuclear Magnetic Resonance . 2018,第期

机译：同时同时同核和异种核旋转在魔法角旋转固态NMR中的去耦
3. Heteronuclear decoupling interference during symmetry-based homonuclear recoupling in solid-state NMR [J] . Marin-Montesinos I, Brouwer DH, Antonioli G, Journal of magnetic resonance . 2005,第2期

机译：固态NMR中基于对称的同核重耦合过程中的异核解耦干扰
4. PREPARATION AND CHARACTERIZATION OF IMAZALIL / β-CYCLODEXTRIN INCLUSION COMPLEX BY SUPERCRITICAL CARBON DIOXIDE AND ~(13)C CP-MAS AND ~1H NMR SPECTROSCOPY: PRELIMINARY RESULTS [C] . Marongiu B., Piras A., Porcedda S., International Symposium on Supercritical Fluids Tome 3: Materials Processing; 20030428-20030430; Versailles; FR . 2003

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5. Quantitative analysis of the Uncompahgre National Forest soil and its extracts by carbon-13 DP- and CP-MAS solid state NMR methods (Colorado). [D] . Keeler, Camille. 2001

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6. Long-Observation-Window Band-Selective Homonuclear Decoupling: Increased Sensitivity and Resolution in Solid-State NMR Spectroscopy of Proteins [O] . Jochem O. Struppe, Chen Yang, Yachong Wang, -1

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7. Broadband homonuclear decoupling in heteronuclear shift correlation NMR spectroscopy [O] . Ad Bax 1983

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High-Field and High-Speed CP-MAS ~(13)C NMR Heteronuclear Dipolar-Correlation Spectroscopy of Solids with Frequency-Switched Lee-Goldburg Homonuclear Decoupling

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