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One-step anodization fabrication and morphology characterization of porous AAO with ideal nanopore arrays

机译:理想纳米孔阵列的多孔AAO一步法阳极氧化制备及形貌表征

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摘要

A fabrication method for one-step anodization of an anodic aluminum oxide (AAO) template with nanopore arrays using pretreated high purity aluminum foil is reported in this article. Morphology of the AAO was characterized by scanning electron microscopy (SEM) and atomic force microscopy (AFM). Results showed that porous AAO with ideal nanopore arrays can be fabricated by one-step anodization fabrication technology on high purity aluminum foil which had been anodized at 45V direct current (DC), in 0℃, 0.5M H{sub}2C{sub}2O{sub}4 solution for 48 hours. The average pore diameter and the interpore distance were 80 nm and 120 nm, respectively. Nanopores in porous AAO had very narrow size distribution and were arranged into hexagonal array. The formation mechanism of nanopore arrays in porous AAO is discussed. Porous AAO with ideal nanopore arrays provide an ideal template for preparation of many one-dimensional nanomaterials. One-step anodization of AAO is a simpler procedure and more applicable in industrial application than the previous two-step anodization technology.
机译:本文报道了一种使用预处理的高纯度铝箔对带有纳米孔阵列的阳极氧化铝(AAO)模板进行一步阳极氧化的制造方法。通过扫描电子显微镜(SEM)和原子力显微镜(AFM)表征了AAO的形态。结果表明,在高纯铝箔上通过一步阳极氧化制造技术,可以在45V直流电(DC),0℃,0.5MH {sub} 2C {sub} 2O阳极氧化的条件下,制备具有理想纳米孔阵列的多孔AAO。 {sub} 4解决方案持续48小时。平均孔径和孔间距分别为80nm和120nm。多孔AAO中的纳米孔具有非常窄的尺寸分布,并排列成六边形阵列。探讨了多孔AAO中纳米孔阵列的形成机理。具有理想纳米孔阵列的多孔AAO为制备许多一维纳米材料提供了理想的模板。与先前的两步阳极氧化技术相比,AAO的一步阳极氧化工艺更简单,并且更适用于工业应用。

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