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ALASCA proficiency testing scheme for occupational hygiene laboratories

机译:ALASCA职业卫生实验室能力验证计划

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摘要

Nowadays, quality assurance is an important part in the environment of analytical laboratories, who need to prove their ability to perform analysis as well to handle routine control as research and development analysis. A proficiency testing scheme (PTS) is one of the possible and powerful tools to evaluate both bias and dispersion of the analysis. As far as industrial hygiene is concerned, since analytical uncertainty is insignificant with regard to sampling strategy uncertainty, laboratories could be tempted to neglect analytical uncertainty assessment as well. The department 'Metrologie des Polluants' (part of INRS) has been organising a proficiency testing scheme since 2002 with the intention of giving the most reliable performance assessment to the participant. The original features, which are also the strong points of the scheme, are: the determination of the assigned value by a method that is independent from the analytical method to be tested; the development of original tools for the fabrication of samples; the strength of the statistic model, which is based on the WASP HSL scheme model; a tool to visualize the results of participants in bias and dispersion contribution; communication with the participants; a completely computerized system to handle the participant database, the sample database, results treatment and report edition; and the use of internet facilities to allow the participant to submit the results via a secured website. All these technical and organisational points are detailed in this paper.
机译:如今,质量保证已成为分析实验室环境中的重要组成部分,分析实验室需要证明自己具有进行分析以及处理常规控制(如研发分析)的能力。能力测试方案(PTS)是评估分析的偏倚和分散的可能且强大的工具之一。就工业卫生而言,由于分析不确定性对于抽样策略不确定性而言微不足道,因此实验室也可能会忽略分析不确定性评估。自2002年以来,“污染大都市”部门一直在组织一项能力测试计划,目的是为参与者提供最可靠的绩效评估。原始特征(也是该方案的强项)是:通过与待测分析方法无关的方法确定分配值;开发用于制作样品的原始工具;基于WASP HSL方案模型的统计模型的强度;可视化参与者偏见和分散贡献结果的工具;与参与者沟通;完全计算机化的系统,用于处理参与者数据库,样本数据库,结果处理和报告版本;以及使用互联网设施允许参与者通过安全的网站提交结果。本文详细介绍了所有这些技术和组织要点。

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