Performance of a horizontal column equipped with a rotary gauze-spring packing was evaluated. Through experiments conducted under atmospheric pressure at total reflux, using the cyclohexane-heptane system, separation efficiency, liquid holdup, and pressure drop were measured. Separation efficiency for the horizontal orientation (at 0 degrees) was somewhat better than at 5 degrees, and was expressed in terms of HETP, which ranged from 0.1 to 0.3 m when F-factor ranged from 0.05 to 0.32 m/s(kg/m(3))(1/2) for a speed of rotation of 100 to 600 rpm. Efficiency of the gauze-spring packing was somewhat inferior to that of the screw-brush packing described in our previous work. However, we found that pressure drop of the former can be reduced to one-tenth that of the latter, corresponding to one-hundredth that of a conventional packed column, such as a column having a Sulzer or McMahon packing. [References: 4]
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机译:评估了装有旋转纱网弹簧填料的卧式色谱柱的性能。通过在大气压下于全回流下进行的实验,使用环己烷-庚烷系统,测量了分离效率,液体保持率和压降。水平方向(0度)的分离效率略好于5度,并以HETP表示,当F因子在0.05至0.32 m / s(kg / m)时范围为0.1至0.3 m (3))(1/2)用于100至600 rpm的转速。纱布弹簧填料的效率比我们先前工作中描述的螺旋刷填料的效率稍差。但是,我们发现前者的压降可降低至后者的十分之一,相当于常规填充塔(例如具有Sulzer或麦克马洪填料的塔)的压力降的一百分之一。 [参考:4]
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