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EDS technique appliance for investigation of laser remelted and alloyed magnesium cast alloys

机译:EDS技术设备,用于研究激光重熔和合金化的镁铸造合金

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Purpose: The paper presents the results of the qualitative and quantitative microanalysis of the chemical composition of the MgAI6Zn1 alloy. Design/methodology/approach: The magnesium alloy has been heat treatment at 505°C for 600 min and ageing at 170°C for 720 min. The study was performed on a transmission electron microscope FEI TITAN company operating at 300kV operating voltage. The qualitative and quantitative microanalysis of the chemica! composition of the Mg alloy microareas was examined using EDS.Findings: Analysis of the results of the concentration of the main alloying elements in the separation test using various magnifications revealed that with an increase in the share of the magnification of the alloying elements. This increase is referred to a linear, the regression coefficient R2, depending on the test element is in the range 0.84-0.97.Practical implications: Tested MgAI6Zn1 alloy can be applied among the others in automotive industry but it requires additional researches.Originality/value: It was demonstrated that the lower magnesium concentration in the EDS results is connected with the increase of magnification induces an effect of X-rays scattering only from the analysed particles and the effect of Mg matrix is limited.
机译:目的:本文介绍了MgAl6Zn1合金化学成分的定性和定量显微分析结果。设计/方法/方法:镁合金已在505°C热处理600分钟,并在170°C进行时效720分钟。该研究是在FEI TITAN公司的透射电子显微镜上进行的,工作电压为300kV。化学成分的定性和定量显微分析!发现:用各种放大倍数对分离试验中主要合金元素浓度的结果进行分析后发现,合金元素放大率的份额增加了。这种增加是线性的,回归系数R2取决于测试元素在0.84-0.97范围内。 :证明EDS结果中较低的镁浓度与放大倍数的增加有关,仅引起X射线从被分析颗粒散射的作用,而Mg基质的作用受到限制。

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