AN EFFICIENT TWO-STEP SYNTHESIS OF 4-METHYL-1,2,3,5,6,10b-HEXAHYDROPYRIMIDO[5,4-c]QUINOLINE-2,5-DIONES VIA BIGINELLI REACTION

Lhassane Ismaili; Sophie Ubaldi; Jean-Francois Robert

首页> 外文期刊>Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry >AN EFFICIENT TWO-STEP SYNTHESIS OF 4-METHYL-1,2,3,5,6,10b-HEXAHYDROPYRIMIDO[5,4-c]QUINOLINE-2,5-DIONES VIA BIGINELLI REACTION

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AN EFFICIENT TWO-STEP SYNTHESIS OF 4-METHYL-1,2,3,5,6,10b-HEXAHYDROPYRIMIDO[5,4-c]QUINOLINE-2,5-DIONES VIA BIGINELLI REACTION

机译：通过比吉内利反应高效地两步合成4-甲基-1,2,3,5,6,10b-己基嘧啶[5,4-c]喹啉-2,5-二酮

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An efficient two-step synthesis of 4-methyl-1,2,3,5,6,10b-hexahydropyrimido[5,4-c]quinoline-2,5-diones is presented.It consists of the reactions of appropriate aldehyde,urea and ethyl acetoacetate according to Biginelli reaction,followed by cyclisation with ammonia.

机译：提出了一种有效的两步合成4-甲基-1,2,3,5,6,10b-六氢嘧啶基[5,4-c]喹啉-2,5-二酮的方法，它由适当的醛，尿素和乙酰乙酸乙酯根据Biginelli反应进行反应，然后与氨环化。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2007年第4期|共8页
作者
Lhassane Ismaili; Sophie Ubaldi; Jean-Francois Robert;
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1. AN EFFICIENT TWO-STEP SYNTHESIS OF 4-METHYL-1,2,3,5,6,10b-HEXAHYDROPYRIMIDO[5,4-c]QUINOLINE-2,5-DIONES VIA BIGINELLI REACTION [J] . Lhassane Ismaili, Sophie Ubaldi, Jean-Francois Robert Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2007,第4期

机译：通过比吉内利反应高效地两步合成4-甲基-1,2,3,5,6,10b-己基嘧啶[5,4-c]喹啉-2,5-二酮
2. Synthesis and antioxidant activity evaluation of new hexahydropyrimido(5,4-c)quinoline-2,5-diones and 2-thioxohexahydropyrimido(5,4-c)quinoline-5-ones obtained by Biginelli reaction in two steps. [J] . Ismaili L, Nadaradjane A, Nicod L, European Journal of Medicinal Chemistry: Chimie Therapeutique . 2008,第6期

机译：通过Biginelli反应分两步获得的新的六氢嘧啶基（5,4-c）喹啉-2,5-二酮和2-硫氧六氢嘧啶基（5,4-c）喹啉-5-酮的合成和抗氧化活性评估。
3. Fast and Efficient One-Pot Three-Component Synthesis of Some 1,2,3,4-Tetrahydro-6-methyl-N-phenyl-5-pyrimidinecarboxamide Derivatives via Biginelli Condensation Reaction [J] . Letters in organic chemistry . 2020,第5期

机译：通过Biginelli缩合反应快速高效的单罐三组分合成一些1,2,3,4-四氢-6-甲基-N-苯基-5-嘧啶羧酰胺衍生物
4. SYNTHESIS AND IN VITRO DEGRADATION OF COPOLYMER OF GLYCOLIDE WITH 6(R,S)-METHYL-MOPHOLINE-2,5-DIONE [C] . Fusheng Du, Weiping Ye, Zhongwei Gu, Asia symposium on polymerization and fine polymers . 1995

机译：6（R，S）-甲基-甲基-2,5-二酮与乙交酯共聚物的合成及体外降解
5. Mechanistic studies on the degradation of gasoline oxygenates by advanced oxidation technologies and the reaction of 4-methyl-1,2,4-triazoline-3,5-dione with tetracyclopropylethylene. [D] . Kim, Duk Kyung. 2003

机译：先进氧化技术降解汽油含氧化合物的机理研究以及4-甲基-1,2,4-三唑啉-3,5-二酮与四环丙基乙烯的反应
6. Efficient synthesis of dihydropyrimidinones via a three-component Biginelli-type reaction of urea alkylaldehyde and arylaldehyde [O] . Haijun Qu, Xuejian Li, Fan Mo, 2013

机译：通过尿素烷基醛和芳醛的三组分Biginelli型反应有效合成二氢嘧啶酮
7. Thermal reaction of 3aH,5H-thiazolo[5,4-c]quinoline-2,4-diones – an easy pathway to 4-amino-1H-quinolin-2-ones and novel 6H-thiazolo[3,4-c]quinazoline-3,5-diones [O] . Vladimír Mrkvička, Antonín Klásek, Roman Kimmel, 2008

机译：3aH，5H-噻唑并[5,4-c]喹啉-2,4-二酮的热反应 - 一种容易通向4-氨基-1H-喹啉-2-酮和新型6H-噻唑并[3,4-c]的途径喹唑啉-3,5-二酮

AN EFFICIENT TWO-STEP SYNTHESIS OF 4-METHYL-1,2,3,5,6,10b-HEXAHYDROPYRIMIDO[5,4-c]QUINOLINE-2,5-DIONES VIA BIGINELLI REACTION

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