Synthesis of the amidite reagent to built bipyridine units into dna backbone

Toshihiro Ihara; Yoshinori Shirasaka; Yoshinobu Sato; Yusuke Kitamura; Kenji Okada; Masato Tazaki; Akinori Jyo

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Synthesis of the amidite reagent to built bipyridine units into dna backbone

机译：合成亚酰胺试剂以将联吡啶单元构建到dna骨架中

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摘要

A new amidite reagent (9) containing 6,6'-bis(acylamino)-2,2'-bipyridine unit was synthesized in moderate yields by a dependable eight step procedure.The unit should work as a metal ion-directed conformational modulator when it is built into the backbone of synthetic DNAs.

机译：通过可靠的八步程序以中等收率合成了一种新的含6,6'-双（酰基氨基）-2,2'-联吡啶单元的亚酰胺试剂（9），该单元应在金属离子定向构象调节剂作用下工作它内置在合成DNA的骨架中。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2005年第2期|共9页
作者
Toshihiro Ihara; Yoshinori Shirasaka; Yoshinobu Sato; Yusuke Kitamura; Kenji Okada; Masato Tazaki; Akinori Jyo;
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1. Synthesis of the amidite reagent to built bipyridine units into dna backbone [J] . Toshihiro Ihara, Yoshinori Shirasaka, Yoshinobu Sato, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2005,第2期

机译：合成亚酰胺试剂以将联吡啶单元构建到dna骨架中
2. Synthesis, characterization, DNA-binding, and DNA-photocleavage properties of (Co(bpy)2(7-NO2-dppz))3+, (Co(dmb)2(7-NO2-dppz))3+, and (Co(phen)2(7-NO2-dppz))3+ complexes: (7-nitro-dppz = 7-nitro dipyrido(3,2-a:2'-3'-c)phenazine; bpy = 2,2'-bipyridine; dmb = 4,4'-dimethyl-2,2'-bipyridine; phen = 1,10-phenanthroline) and their toxicity on different microorganisms. [J] . Reddy KL, Reddy YH, Kumar KA, Nucleosides, nucleotides and nucleic acids . 2009,第3期

机译：（Co（bpy）2（7-NO2-dppz））3 +，（Co（dmb）2（7-NO2-dppz））3+和（的合成，表征，DNA结合和DNA光解性质Co（phen）2（7-NO2-dppz））3+配合物：（7-硝基-dppz = 7-硝基二吡啶（3,2-a：2'-3'-c）吩嗪; bpy = 2,2 '-联吡啶; dmb = 4,4'-二甲基-2,2'-联吡啶; phen = 1,10-菲咯啉）及其对不同微生物的毒性。
3. Synthesis, DNA binding, and DNA photocleavage of the ruthenium(II) complexes [Ru(bpy)(btip)](2+) and [Ru(dmb)(btip)](2+) (bpy=2,2 '-bipyridine; btip=2-benzo[b]thien-2-yl-1H-imidazo[4,5-f] [1,10]phenanthroline; dmb=4,4 '-dimethyl-2,2 '-bipyridine) [J] . Tan LF, Wang F, Chao H Helvetica chimica acta . 2007,第1期

机译：钌（II）配合物[Ru（bpy）（btip）]（2+）和[Ru（dmb）（btip）]（2+）的合成，DNA结合和DNA光裂解（bpy = 2,2'-联吡啶; btip = 2-苯并[b]噻吩-2-基-1H-咪唑并[4,5-f] [1,10]菲咯啉; dmb = 4,4'-二甲基-2,2'-联吡啶
4. Synthesis and Characterization of 6,6'-bis(2-hydroxyphenyl)-2,2'-bipyridine ligand and Its Interaction with ct-DNA [C] . Norhidayah Selamat, Lee Yook Heng, Nurul Izzaty Hassan, UKM FST Postgraduate Colloquium . 2015

机译：6,6'-BIS（2-羟基苯基）-2,2'-硼吡啶配体的合成与表征及其与CT-DNA的相互作用
5. Synthesis and study of rigidified nucleosides analogues for probing the importance of the deoxyribose DNA backbone. [D] . Yueh, Han. 2012

机译：合成和研究刚性核苷类似物，以探讨脱氧核糖DNA主链的重要性。
6. A Selective Sensor for Silver Ions Built From Polyfluorophores on a DNA Backbone [O] . Samuel S. Tan, Yin Nah Teo, Eric T. Kool -1

机译：选择性传感器的银离子内置从polyfluorophores在DNa骨架
7. Hairpin-shaped DNA duplexes with disulfide bonds in sugar-phosphate backbone as potential DNA reagents for crosslinking with proteins [O] . Dolinnaya Nina, Metelev Valeri, Oretskaya Tatiana, 1999

机译：糖-磷酸骨架中带有二硫键的发夹状DNA双链体，作为潜在的与蛋白质交联的DNA试剂
8. Synthesis and Ab Initio Structure Determination of Zn4O(BO3)2, a Microporous Zincoborate Built Up From 'Fused' 3-Ring and 5-Ring Sub-Units. [R] . Harrison, W. T., Gier, T. E., Stucky, G. D. 1993

机译：Zn4O（BO3）2的合成和从头构型测定，由“稠合”3环和5环亚单元构成的微孔硼酸盐。

Synthesis of the amidite reagent to built bipyridine units into dna backbone

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