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Optimization of Microwave Drying Biomass Material of Stem Granules from Waste Tobacco Using Response Surface Methodology

机译:响应面法优化微波法干燥废旧烟梗颗粒生物质

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Tobacco stems, an underutilized waste in the tobacco industry, can be transformed into a viable product through the preparation of biomass material of stem granules. Response surface methodology (RSM) was used to optimize microwave drying of stem granules from waste tobacco. The effects of microwave power (35-40 kW), moisture content (25-35%), material thickness (30-50 mm), and drying time (90-150 s) on filling power and yield of stem granules were studied. Gas chromatography-mass spectroscopy (GC-MS) and scanning electron microscopy (SEM) were used to determine volatile components and microstructures of stem granules dried under optimal conditions. The filling power and yield of stem granules could be adequately fitted to a quadratic model (R~2 = 0.951) and a two-factor interaction model (R~2 = 0.887), respectively. The optimal conditions for microwave drying of stem granules were 35 kW, 30%, 30 mm, and 150 s. When prepared under optimal conditions, the filling power and yield of stem granules were 7.94 cm~3/g and 64.06%, respectively, which differed by only 4.53 and 3.50% from model predictions. The quadratic and two-factor interaction models provided a reasonably accurate (<5% error) assessment of optimal conditions for microwave drying of biomass material of stem granules from waste tobacco stems.
机译:烟梗是烟草业中未被充分利用的废物,可通过制备烟梗颗粒的生物质材料将其转化为可行的产品。响应表面方法(RSM)用于优化微波干燥废烟梗颗粒。研究了微波功率(35-40 kW),水分含量(25-35%),材料厚度(30-50 mm)和干燥时间(90-150 s)对茎粒填充力和产量的影响。气相色谱-质谱(GC-MS)和扫描电子显微镜(SEM)用于确定在最佳条件下干燥的茎干颗粒的挥发性成分和微观结构。茎粒的填充力和产量可以分别拟合为二次模型(R〜2 = 0.951)和两因素相互作用模型(R〜2 = 0.887)。茎干颗粒微波干燥的最佳条件是35 kW,30%,30 mm和150 s。在最佳条件下制备,茎干颗粒的填充力和得率分别为7.94 cm〜3 / g和64.06%,与模型预测的相差仅4.53%和3.50%。二次和两因素相互作用模型为微波干燥废烟茎秆颗粒中生物质材料的最佳条件提供了合理准确的评估(误差小于5%)。

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