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Improvements in MMC coatings - influence of powder preparation (mixture or ball milling) and powder size on the coating behavior

机译:MMC涂层的改进-粉末制备(混合物或球磨)和粉末尺寸对涂层性能的影响

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摘要

Metal-Matrix Composites (MMC) are composed of hard particles that exhibit exceptional wear resistance. In this way, many investigations were conducted to improve the life span of structures. Regarding surface stress, thermal spraying can be appropriate to elaborate thick composite coatings with specific behaviour. In order to improve coating mechanical properties, it is necessary to manufacture samples with more homogeneous microstructures. Thus, the chosen approach was to optimize the powder morphology through mechanical alloying. Indeed, when mechanical alloying process is used to synthesize composite powders strengthened by particle dispersion, powders tend to fracture into small segments, especially when a high content of hard particles is added. Powder microstructures are then refined which induces thinner coating morphology and reduces their porosity content. In the present work, the mechanical alloying (ball milling) method was developed to synthesize NiCrBSi-WC composite powders using HVOF. Considering different granular sizes of powders (micrometric and nanometric) after parameter optimization, composite coatings were compared with standard coatings elaborated from mixed powders. SEM observations, hardness measurements, DRX analysis were the first technologies implemented to characterize Metal Matrix Composite coatings.
机译:金属基复合材料(MMC)由具有出色耐磨性的硬质颗粒组成。以此方式,进行了许多研究以改善结构的寿命。关于表面应力,热喷涂可适合于制成具有特定性能的厚复合涂层。为了改善涂层的机械性能,有必要制造具有更均匀的微观结构的样品。因此,选择的方法是通过机械合金化来优化粉末形态。实际上,当使用机械合金化工艺来合成通过颗粒分散增强的复合粉末时,粉末往往会破裂成小段,特别是当添加大量硬颗粒时。然后细化粉末的微观结构,这会导致更薄的涂层形态并降低其孔隙率。在目前的工作中,开发了机械合金化(球磨)方法以使用HVOF合成NiCrBSi-WC复合粉末。考虑到参数优化后粉末的不同粒度(微米和纳米),将复合涂层与由混合粉末制成的标准涂层进行了比较。 SEM观察,硬度测量,DRX分析是用于表征金属基复合材料涂层的首批技术。

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