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Characteristics and heat treatment of cold-sprayed Al-Sn binary alloy coatings

机译:冷喷涂Al-Sn二元合金涂层的特性和热处理

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摘要

In this study, Al-Sn binary alloy coatings were prepared with Al-5wt.%Sn (Al-5Sn) and Al-10wt.%Sn (Al-10Sn) gas atomized powders by low pressure and high-pressure cold spray process. The microstructure and microhardness of the coatings were characterized. The as-sprayed coating were heat treated at 150, 200, 250 and 300℃ for 1 hour, respectively. The effect of heat treatment on microstructure, microhardness and conten of Sn phase of the coatings were investigated. The bonding strength of as-sprayed and heat treated Al-Sn coatings were also studied. The results show that the dense and well-bonded Al-10Sn coating can be deposited by low pressure with helium gas while Al-5Sn coating by high-pressure cold spray with nitrogen gas. The content of Sn for both Al-5Sn and Al-10Sn in as-sprayed coatings are consistent with that in feed stock powders. The coarsening and/or migration of Sn phase in both coatings were observed when the annealing temperature exceeds 200℃. Furthermore, the microhardness of the coatings decreased significantly under the annealing temperature of 250℃. EDAX analysis shows that the heat treatment has no significant effect on content of Sn phase in Al-5Sn coatings. Bonding strength of as-sprayed Al-10Sn coating is slightly higher than that of Al-5Sn coating. Annealing under 200℃ can increase the bonding strength of Al-5Sn coatings.
机译:在这项研究中,通过低压和高压冷喷涂工艺,用Al-5wt。%Sn(Al-5Sn)和Al-10wt。%Sn(Al-10Sn)气体雾化粉末制备了Al-Sn二元合金涂层。表征了涂层的显微组织和显微硬度。喷涂后的涂层分别在150、200、250和300℃下热处理1小时。研究了热处理对涂层组织,显微硬度和Sn相含量的影响。还研究了喷涂和热处理后的Al-Sn涂层的结合强度。结果表明,致密且粘结良好的Al-10Sn涂层可以在低压下用氦气沉积,而Al-5Sn涂层可以在高压下用氮气进行冷喷涂。喷涂涂层中的Al-5Sn和Al-10Sn中的Sn含量与原料粉末中的含量一致。当退火温度超过200℃时,在两个涂层中都观察到了Sn相的粗化和/或迁移。此外,在250℃的退火温度下,涂层的显微硬度明显降低。 EDAX分析表明,热处理对Al-5Sn涂层中Sn相含量没有明显影响。喷涂后的Al-10Sn涂层的结合强度略高于Al-5Sn涂层。 200℃退火可以提高Al-5Sn涂层的结合强度。

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