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Characteristics And Heat Treatment Of Cold-sprayed Al-sn Binary Alloy Coatings

机译:冷喷涂Al-sn二元合金涂层的特性和热处理

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In this study, Al-Sn binary alloy coatings were prepared with Al-5 wt.% Sn (Al-5Sn) and Al-10 wt.% Sn (Al-10Sn) gas atomized powders by low pressure and high pressure cold spray process. The microstructure and microhardness of the coatings were characterized. To understand the coarsening of tin in the coating, the as-sprayed coatings were annealed at 150, 200, 250 and 300 ℃ for 1 h, respectively. The effect of annealing on microstructure and the bond strength of the coatings were investigated. The results show that Al-5Sn coating can be deposited by high pressure cold spray with nitrogen while Al-10Sn can only be deposited by low pressure cold spray with helium gas. Both Al-5Sn and Al-10Sn coatings present dense structures. The fraction of Sn in as-sprayed coatings is consistent with that in feed stock powders. The coarsening and/or migration of Sn phase in the coatings were observed when the annealing temperature exceeds 200 ℃. Furthermore, the microhardness of the coatings decreased significantly at the annealing temperature of 250 ℃. EDXA analysis shows that the heat treatment has no significant effect on fraction of Sn phase in Al-5Sn coatings. Bonding strength of as-sprayed Al-10Sn coating is slightly higher than that of Al-5Sn coating. Annealing at 200 ℃ can increase the bonding strength of Al-5Sn coatings.
机译:在这项研究中,通过低压和高压冷喷涂工艺,用Al-5 wt。%的Sn(Al-5Sn)和Al-10 wt。%的Sn(Al-10Sn)气体雾化粉末制备了Al-Sn二元合金涂层。表征了涂层的显微组织和显微硬度。为了理解涂层中锡的粗化,将喷涂后的涂层分别在150、200、250和300℃下退火1小时。研究了退火对涂层微观组织和结合强度的影响。结果表明,Al-5Sn涂层可通过氮气高压冷喷涂沉积,而Al-10Sn只能通过氦气低压冷喷涂沉积。 Al-5Sn和Al-10Sn涂层都具有致密的结构。喷涂涂层中锡的含量与原料粉末中的含量一致。当退火温度超过200℃时,观察到涂层中锡相的粗大化和/或迁移。此外,在250℃的退火温度下,涂层的显微硬度明显降低。 EDXA分析表明,热处理对Al-5Sn涂层中的Sn相含量没有明显影响。喷涂后的Al-10Sn涂层的结合强度略高于Al-5Sn涂层。 200℃退火可以提高Al-5Sn涂层的结合强度。

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