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Strain-Rate Sensitivity of the Hardness of Crystalline Materials under Dynamic Nanoindentation

机译:动态纳米压痕作用下结晶材料硬度的应变率敏感性

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The coefficients of the strain-rate sensitivity of plastic characteristics (including microhardness) carry useful information concerning the nature of elementary carriers of plastic deformation and their mobility in a solid. In macrotests of various ductile materials (see, e.g., [1]), a wide range of strain rates ε (between 10~(-8) and 10~6 s~(-1)) was investigated. However, fracture of many brittle materials (in particular, single crystals with covalent bonds, ceramics, glasses, etc.) begins before noticeable plastic strain. The plastic properties of such materials are usually studied by the methods of local deformation or microindentation. In recent years, the method of nanoindentation has also been extensively used in this field [2-4]. Famous firms (MTS, Micromaterials, CSEM, Hysitron, etc.) produce commercial nanotesters only for small ε values (10~(-3) - 10~(-1)s~(-1)). At the same time, very high rates of local deformation in submicron areas (10~(-1) s~(-1)) are characteristic for many processes, including dry friction between rough surfaces, abrasive and erosive wear, atomic-force microscopy, nanolithography by the methods of imprinting and scribing, and fine grinding [5]. Thus, the area of the mechanical properties of materials that is characterized by both short loading time intervals and small deformation zones is little studied. Under these conditions, the ordinary mechanisms (in particular, dislocation mechanisms) of plastic flow can be strongly impeded or suppressed.
机译:塑性特性(包括显微硬度)的应变率敏感性系数载有关于塑性变形基本载体的性质及其在固体中的迁移性的有用信息。在各种延展性材料的宏观测试中(例如参见[1]),研究了大范围的应变率ε(在10〜(-8)和10〜6 s〜(-1)之间)。但是,许多脆性材料(特别是具有共价键的单晶,陶瓷,玻璃等)的断裂在明显的塑性应变之前就开始了。通常通过局部变形或微压痕的方法研究这种材料的塑性。近年来,纳米压痕方法也被广泛用于该领域[2-4]。著名公司(MTS,微材料,CSEM,Hysitron等)仅针对较小的ε值(10〜(-3)-10〜(-1)s〜(-1))生产商业纳米测试仪。同时,在许多过程中,亚微米区域的局部变形率很高( 10〜(-1)s〜(-1)),包括粗糙表面之间的干摩擦,磨料和侵蚀性磨损,力显微镜,通过压印和划刻的方法进行纳米平版印刷以及精细研磨[5]。因此,很少研究以加载时间间隔短和变形区小为特征的材料的机械性能区域。在这些条件下,可以强烈地阻碍或抑制塑性流动的普通机制(特别是位错机制)。

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