Crystal structure of bis(u2-thiocyanato)tetrakis(3,5-dimethyl-l-(thiocarbamoyl)pyrazole)dinickel(II) dichloride ethanol disolvate, [Ni(NCS)_2(C_6H_6N_3S)_4][Cl]_2·2C_2H_5OH

摘要

The complex was synthesized by mixing hot ethanolic solution of the ligand 3,5-dimethyl-l-thiocarboxamide pyrazole (Pz-CS, 1 mmol) and NiCk 6H2O (0.5 mmol). The solution was filtered and the filtrate left to crystallize. The precipitated crystals were separated by filtration.