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Regenerated cellulose/graphene nanocomposite films prepared in DMAC/LiCl solution

机译:在DMAC / LiCl溶液中制备的再生纤维素/石墨烯纳米复合薄膜

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Regenerated cellulose/graphene composite films had been prepared by dispersing graphene into cellulose solution in DMAC/LiCl, and then casting the solution onto glass. The thermal stability and mechanical properties of the composite materials, compared with pure regenerated cellulose film, were significandy improved. When the graphene loading was only 0.4 wt.%, the 10% weight loss temperature increased 20 C. The Young's modulus increased from 3.4 to 7.2 GPa, while tensile strength increased from 89 to 148 MPa when 1.6 wt.% graphene was added into cellulose film. The electrical conductivity of the nanocomposite film reached 3.7 x 10~(-6) S/cm when 1.6 wt.% graphene was incorporated. The morphology was investigated by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The images revealed that the graphene was nano-dispersed in cellulose matrix. The effect of the graphene content in the nanocomposite material was also investigated.
机译:通过将石墨烯分散到DMAC / LiCl中的纤维素溶液中,然后将溶液浇铸到玻璃上,可以制备再生的纤维素/石墨烯复合膜。与纯再生纤维素膜相比,复合材料的热稳定性和机械性能得到了显着改善。当石墨烯的负载量仅为0.4 wt。%时,失重10%的温度增加20°C。当向纤维素中添加1.6 wt。%的石墨烯时,杨氏模量从3.4 GPa增加到7.2 GPa,而拉伸强度从89 MPa增加到148 MPa。电影。当掺入1.6重量%的石墨烯时,纳米复合膜的电导率达到3.7×10 6(-6)S / cm。通过扫描电子显微镜(SEM)和透射电子显微镜(TEM)研究了形态。图像显示石墨烯被纳米分散在纤维素基质中。还研究了纳米复合材料中石墨烯含量的影响。

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