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Study of sol-gel process for preparing cerium nano-oxide films on AA7020-T6 Al alloy

机译:AA7020-T6铝合金溶胶-凝胶法制备铈纳米氧化物膜的研究

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摘要

A design of experiment technique, the Taguchi method, has been used to optimise a coating process in order to decrease the corrosion rate and increase the passivity of the coated samples by controlling the coating process's factors. Potentiodynamic polarisation measurements were carried out to determine the corrosion rate and passivity of the coated samples. The optimised coating parameters for corrosion rate are one molar ratio for acid citric/CeCI_3, 300 deg C for heat treatment temperature, 0.02 mol for CeCI_3 concentration and 0 min for time of boiling. The optimised coating parameters for passive region are two molar ratio for acid citric/CeCI_3, 300 deg C for heat treatment temperature, 0.001 mol for CeCI_3 concentration and 60 min for time of boiling. The results showed that the acid citric/CeCI_3 is the most significant factor affecting the corrosion rate while the time of boiling affects significantly on the passive region of the coatings.
机译:实验技术的设计,即Taguchi方法,已用于优化涂层工艺,以便通过控制涂层工艺的因素来降低腐蚀速率并提高涂层样品的钝化率。进行电位动力学极化测量以确定涂层样品的腐蚀速率和钝化率。优化的腐蚀速率涂层参数为:柠檬酸/ CeCl_3的摩尔比,热处理温度为300℃,CeCl_3浓度为0.02 mol和沸腾时间为0分钟。钝化区的最佳涂层参数为:柠檬酸/ CeCl_3的两个摩尔比,热处理温度为300℃,CeCl_3浓度为0.001 mol和沸腾时间为60分钟。结果表明,柠檬酸/ CeCI_3是影响腐蚀速率的最重要因素,而沸腾时间对涂层的钝化区域有显着影响。

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