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The use of argon cluster bombardment for the surface preparation of paint cross-sections for analysis by ToF-SIMS

机译:氩气团轰击在油漆横截面表面制备中的应用,以用于ToF-SIMS分析

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摘要

Surface preparation with gas cluster ion beam (GCIB) sputtering was performed on paint cross-sections, which belong to the collection of the Royal Institute for Cultural Heritage (KIKIRPA), Brussels, Belgium. Superficial cleaning of cross sectionswith residual embedding resin surface contamination was studied with different sputtering times in order to obtain a gain in the spectral and imaging mode. Sputtering was made directly through the Time-of-Flight-SIMS apparatus. It was thus demonstrated that GCIB sputtering for a short periodwas very efficient for the superficial decontamination of cultural heritage cross-sections without visible damage on the valuable samples. The GCIB sputtering time and dose can be highly decreased when combined with a monoatomic argon ion beam preparation techniques such as the ion milling systems.
机译:气体横截面离子束(GCIB)溅射的表面处理是在油漆横截面上进行的,该横截面属于比利时布鲁塞尔皇家文化遗产研究所(KIKIRPA)的收藏。为了获得光谱和成像模式的增益,研究了在不同的溅射时间对残留的嵌入树脂表面污染的表面进行表面清洁。通过飞行时间-SIMS设备直接进行溅射。因此证明,短时间GCIB溅射对于文化遗产横截面的表面净化非常有效,而对有价值的样品没有明显的损害。当与单原子氩离子束制备技术(例如离子铣削系统)结合使用时,可以大大降低GCIB的溅射时间和剂量。

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